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Chemical Structure| 19293-63-1 Chemical Structure| 19293-63-1

Structure of 19293-63-1

Chemical Structure| 19293-63-1

Dicyclohexylmethanamine

CAS No.: 19293-63-1

4.5 *For Research Use Only !

Cat. No.: A651545 Purity: 95%

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Product Details of [ 19293-63-1 ]

CAS No. :19293-63-1
Formula : C13H25N
M.W : 195.34
SMILES Code : NC(C1CCCCC1)C2CCCCC2
MDL No. :MFCD12154076
InChI Key :QVQGTNFYPJQJNM-UHFFFAOYSA-N
Pubchem ID :10774245

Safety of [ 19293-63-1 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H314-H335
Precautionary Statements:P260-P264-P271-P280-P301+P330+P331-P303+P361+P353-P305+P351+P338-P308+P311-P338-P363-P403+P233-P405-P501
Class:8
UN#:2735
Packing Group:

Application In Synthesis of [ 19293-63-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 19293-63-1 ]

[ 19293-63-1 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 328-72-3 ]
  • [ 32673-25-9 ]
  • [ 19293-63-1 ]
  • [ 107-13-1 ]
  • [ 1027717-63-0 ]
YieldReaction ConditionsOperation in experiment
69% With NBu4Br;palladium diacetate; In ISOPROPYLAMIDE; water; Example 16 Synthesis of 3,5-bis(trifluoromethyl)cinnamonitrile 0.382 g (7.2 mmol) of acrylonitrile, 38.7 mg (120 mumol) of NBu4Br, 6.7 mg (30 mumol) of palladium acetate and 26.7 mg (120 mumol) of phenyldi(t-butyl)phosphine are weighed into a Schlenk vessel. 1.49 g (6 mmol) of <strong>[328-72-3]3,5-bis(trifluoromethyl)chlorobenzene</strong> and 1.53 ml (7.2 mmol) of dicyclohexylmethylamine and also 3.5 ml of dimethylacetamide are then added. The Schlenk vessel is placed in a heating bath at 130 C. and the contents are stirred. After 4 hours, the contents are poured into 30 ml of water and the product is extracted by shaking with t-butyl methyl ether. After drying the organic phase over MgSO4, the solvent is removed under reduced pressure and the product is isolated. Orange oil, yield: 69%.
  • 2
  • [ 328-72-3 ]
  • [ 32673-25-9 ]
  • [ 19293-63-1 ]
  • [ 79-06-1 ]
  • 3,5-bis(trifluoromethyl)cinnamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
With NBu4Br;palladium diacetate; In ISOPROPYLAMIDE; water; Example 9 Synthesis of 3,5-bis(trifluoromethyl)cinnamide (Method I) 0.512 g (7.2 mumol) of acrylamide, 38.7 mg (120 mumol) of NBu4Br, 6.7 mg (30 mumol) of palladium acetate and 26.7 mg (120 mumol) of phenyldi(t-butyl)phosphine are weighed into a Schlenk vessel. 1.49 g (6 mmol) of <strong>[328-72-3]3,5-bis(trifluoromethyl)chlorobenzene</strong> and 1.53 ml (7.2 mmol) of dicyclohexylmethylamine and also 3.5 ml of dimethylacetamide are then added. The Schlenk vessel is placed in a heating bath at 130 C. and the contents are stirred. After 4 hours, the contents are poured into 30 ml of water, the solid product is filtered off with suction and washed with about 50 ml of water. Light-grey solid, yield after drying: 1.63 g (96% of theory).
With NBu4Br;palladium diacetate; In ISOPROPYLAMIDE; Example 10 Synthesis of 3,5-bis(trifluoromethyl)cinnamide (Method II) 0.181 g (2.55 mmol) of acrylamide, 9.7 mg (30 mumol) of NBu4Br, 0.675 mg (3 mumol) of palladium acetate and 2.67 mg (12 mumol) of phenyldi(t-butyl)phosphine are weighed into a Schlenk vessel. 0.542 g (3 mmol) of <strong>[328-72-3]3,5-bis(trifluoromethyl)chlorobenzene</strong> and 0.637 ml (3 mmol) of dicyclohexylmethylamine and also 2.5 ml of dimethylacetamide are then added. The Schlenk vessel is placed in a heating bath at 130 C. and the contents are stirred. After 3 hours, the yield is determined by means of HPLC: 99% (TON=723, TOF=241/h).
  • 3
  • [ 328-72-3 ]
  • [ 32673-25-9 ]
  • [ 19293-63-1 ]
  • [ 292638-85-8 ]
  • [ 705250-77-7 ]
YieldReaction ConditionsOperation in experiment
With NBu4Br;palladium diacetate; In ISOPROPYLAMIDE; water; Example 13 Synthesis of Methyl 3,5-bis(trifluoromethyl)cinnamate 0.619 g (7.2 mmol) of methyl acrylate, 38.7 mg (120 mumol) of NBu4Br, 6.7 mg (30 mumol) of palladium acetate and 26.7 mg (120 mumol) of phenyldi(t-butyl)phosphine are weighed into a Schlenk vessel. 1.49 g (6 mmol) of <strong>[328-72-3]3,5-bis(trifluoromethyl)chlorobenzene</strong> and 1.53 ml (7.2 mmol) of dicyclohexylmethylamine and also 3.5 ml of dimethylacetamide are then added. The Schlenk vessel is placed in a heating bath at 130 C. and the contents are stirred. After 4 hours, the contents are poured into 30 ml of water and the product is extracted by shaking with t-butyl methyl ether. After drying the organic phase over MgSO4, the solvent is removed under reduced pressure and the product is isolated. Yellowish, crystalline solid, yield: 1.34 g (97% of theory).
 

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