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Chemistry
Organic Building Blocks
Aryls
nitrophenyl
4-Nitrophenyl trifluoromethanesulfonate
Chemistry
Organic Building Blocks
Aryls
Fluorinated Building Blocks Nitroes Trifluoromethyls Sulfonates Benzene Compounds
nitrophenyl
Alternatived Products of [ 17763-80-3 ]
Product Citations

Product Citations

Jang, Mingyeong ; Lim, Taeho ; Park, Byoung Yong , et al. DOI: PubMed ID:

Abstract: In this study, we developed a metal-free and highly chemoselective method for the reduction of aromatic nitro compounds. This reduction was performed using tetrahydroxydiboron [B2(OH)4] as the reductant and 4,4'-bipyridine as the organocatalyst and could be completed within 5 min at room temperature. Under optimal conditions, nitroarenes with sensitive functional groups, such as vinyl, ethynyl, carbonyl, and halogen, were converted into the corresponding anilines with excellent selectivity while avoiding the undesirable reduction of the sensitive functional groups.

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Product Details of [ 17763-80-3 ]

CAS No. :17763-80-3 MDL No. :MFCD00192354
Formula : C7H4F3NO5S Boiling Point : -
Linear Structure Formula :- InChI Key :NDTIXHNCNLKURN-UHFFFAOYSA-N
M.W : 271.17 Pubchem ID :549870
Synonyms :

Safety of [ 17763-80-3 ]

Signal Word:Danger Class:8
Precautionary Statements:P280-P305+P351+P338-P310 UN#:3261
Hazard Statements:H314 Packing Group:Ⅲ
GHS Pictogram:

Application In Synthesis of [ 17763-80-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 17763-80-3 ]

[ 17763-80-3 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 110-89-4 ]
  • [ 17763-80-3 ]
  • [ 6574-15-8 ]
Reference： [1]Synthesis,1990,p. 1145 - 1147
[2]Synlett,1999,p. 1559 - 1562
[3]Organic Letters,2004,vol. 6,p. 985 - 987
[4]Journal of Organic Chemistry,2000,vol. 65,p. 1158 - 1174
  • 2
  • [ 17763-80-3 ]
  • [ 868755-79-7 ]
Reference： [1]Bioorganic and Medicinal Chemistry Letters,2012,vol. 22,p. 1397 - 1401
  • 3
  • zinc cyanide [ No CAS ]
  • [ 17763-80-3 ]
  • [ 33513-42-7 ]
  • [ 21962-49-2 ]
YieldReaction ConditionsOperation in experiment
With tetrakis(triphenylphosphine) palladium(0); at 110℃; for 8h; Step B: 4-Formyl-2-methoxybenzonitrile: A mixture of the sulfonate (37.0 g, 130 mmol), zinc cyanide (61.1 g, 521 mmol) and tetrakis triphenyiphosphine palladium (0) (22.57 g, 19.53 mmol) in DMF (300 mL) were stirred at 110 C for 8 hr. EtOAc was added to the reaction mixture and the organic layer was washed two times with water, dried, filtered and concentrated. The crude product was then purified by column chromatography (silica gel, ethylacetate/hexanes 3:7) whichafforded the title compound: LC/MS: (IE, m/z) [M + 1] = 162.34.
Reference： [1]Patent: WO2014/99633,2014,A2 .Location in patent: Page/Page column 70

Tags: 17763-80-3 synthesis path| 17763-80-3 SDS| 17763-80-3 COA| 17763-80-3 purity| 17763-80-3 application| 17763-80-3 NMR| 17763-80-3 COA| 17763-80-3 structure

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Technical Information

• Alkyl Halide Occurrence • Benzylic Oxidation • Birch Reduction • Blanc Chloromethylation • Friedel-Crafts Reaction • Hydrogenolysis of Benzyl Ether • Nucleophilicity of Sulfur Compounds • Preparation of Alkylbenzene • Reactions of Benzene and Substituted Benzenes • Vilsmeier-Haack Reaction
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