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Chemical Structure| 39161-84-7 Chemical Structure| 39161-84-7

Structure of 39161-84-7

Chemical Structure| 39161-84-7

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Product Details of [ 39161-84-7 ]

CAS No. :39161-84-7
Formula : C8H8O2S
M.W : 168.21
SMILES Code : O=C(O)CC1=CC=C(S)C=C1
MDL No. :MFCD00797617
InChI Key :ORXSLDYRYTVAPC-UHFFFAOYSA-N
Pubchem ID :3390511

Safety of [ 39161-84-7 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H315-H318-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340+P312-P305+P351+P338-P310-P332+P313-P362-P403+P233-P405-P501
Class:9
UN#:3335
Packing Group:

Application In Synthesis of [ 39161-84-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 39161-84-7 ]

[ 39161-84-7 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 53595-65-6 ]
  • [ 39161-84-7 ]
  • [ 63032-09-7 ]
YieldReaction ConditionsOperation in experiment
With potassium hydroxide; In N-methyl-acetamide; water; Step A: Preparation of 5-(4-carboxymethylphenylthio)thiophene-2-sulfonamide 4-Mercaptophenylacetic acid (2.3 g) was dissolved in dimethylformamide under a nitrogen atmosphere and 1.8 g of potassium hydroxide dissolved in a minimum amount of water was added. 5-bromothiophene-2-sulfonamide (3.3 g) dissolved in dimethylformamide was added and the mixture heated at 120 C. for 2 hours. After cooling to room temperature water was added to the reaction mixture, the pH was adjusted to 8.6 and the mixture was extracted with ethyl acetate. The aqueous phase was separated and acidified, causing a solid to precipitate. The solid was collected by filtration and dried under vacuum to a weight of 3.25 g.
With potassium hydroxide; In N-methyl-acetamide; water; Step A: Preparation of 5-(4-carboxymethylphenylthio)thiophene-2-sulfonamide 4-Mercaptophenylacetic acid (2.3 g) was dissolved in dimethylformamide under a nitrogen atmosphere and 1.8 g of potassium hydroxide dissolved in a minimum amount of water was added. 5-bromothiophene-2-sulfonamide (3.3 g) dissolved in dimethylformamide was added and the mixture heated at 120C for 2 hours. After cooling to room temperature water was added to the reaction mixture, the pH was adjusted to 8.6 and the mixture was extracted with ethyl acetate. The aqueous phase was separated and acidified, causing a solid to precipitate. The solid was collected by filtration and dried under vacuum to a weight of 3.25 g.
  • 2
  • 2-(6-(dimethylamino)-3-(dimethyliminio)-3H-xanthen-9-yl)benzoate [ No CAS ]
  • [ 29022-11-5 ]
  • [ 39161-84-7 ]
  • [ 92122-45-7 ]
  • [ 35661-38-2 ]
  • [ 35661-60-0 ]
  • [ 86123-10-6 ]
  • [ 71989-33-8 ]
  • [ 71989-28-1 ]
  • [ 71989-14-5 ]
  • [ 104091-08-9 ]
  • [ 71989-31-6 ]
  • Nα-fmoc-N(im)-trityl-D-histidine [ No CAS ]
  • 1-tert-butoxycarbonyl-N-[(9-fluorenyl)methoxycarbonyl]-D-tryptophan [ No CAS ]
  • Fmoc-D-Gln(Trt)-OH [ No CAS ]
  • Fmoc-D-Ile-OH [ No CAS ]
  • N-α-[(9H-fluoren-9-ylmethoxy)carbonyl]-NG-(2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl)-D-arginine [ No CAS ]
  • ent-(X1-GGIEMKPHPWFFGKIPRAKAEEMLSKQRHDG-X2); X1=tetramethylrhodamine; X2=[4-(carboxymethyl)phenyl]sulfanyl [ No CAS ]
 

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Technical Information

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[ 39161-84-7 ]

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