Home Cart Sign in  
Chemical Structure| 36646-78-3 Chemical Structure| 36646-78-3

Structure of 36646-78-3

Chemical Structure| 36646-78-3

5,5-Dimethyl-3-(p-tolylamino)cyclohex-2-enone

CAS No.: 36646-78-3

4.5 *For Research Use Only !

Cat. No.: A710134 Purity: 95%

Change View

Size Price

US Stock

Global Stock

In Stock
250mg łËËͶÊÊ Inquiry 1-2 weeks

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • 250mg

    łËËͶÊÊ

In Stock

- +

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 36646-78-3 ]

CAS No. :36646-78-3
Formula : C15H19NO
M.W : 229.32
SMILES Code : O=C1C=C(NC2=CC=C(C)C=C2)CC(C)(C)C1
MDL No. :MFCD00128470

Safety of [ 36646-78-3 ]

Application In Synthesis of [ 36646-78-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 36646-78-3 ]

[ 36646-78-3 ] Synthesis Path-Downstream   1~7

  • 1
  • [ 106-38-7 ]
  • [ 873-95-0 ]
  • [ 36646-78-3 ]
  • 2
  • [ 98-03-3 ]
  • [ 17115-51-4 ]
  • [ 36646-78-3 ]
  • [ 1265632-09-4 ]
YieldReaction ConditionsOperation in experiment
59% at 90℃; for 10h;Neat (no solvent); Aldehyde 1 (1 mmol), dihydrothiophen-3(2H)-one-1,1-dioxide 2 (0.134 g, 1 mmol), enaminone 3 (1 mmol) and were triturated together in an agate mortar for 5 minutes. Then the mixture was kept at 90 C for a certain time (monitored by TLC). The result mixture was washed with water and recrystallized from ethanol (95 %) to give pure product 4.
  • 3
  • [ 17115-51-4 ]
  • [ 36646-78-3 ]
  • [ 459-57-4 ]
  • [ 1265632-05-0 ]
YieldReaction ConditionsOperation in experiment
80% at 90℃; for 9h;Neat (no solvent); Aldehyde 1 (1 mmol), dihydrothiophen-3(2H)-one-1,1-dioxide 2 (0.134 g, 1 mmol), enaminone 3 (1 mmol) and were triturated together in an agate mortar for 5 minutes. Then the mixture was kept at 90 C for a certain time (monitored by TLC). The result mixture was washed with water and recrystallized from ethanol (95 %) to give pure product 4.
  • 4
  • [ 17115-51-4 ]
  • [ 36646-78-3 ]
  • [ 123-11-5 ]
  • [ 1265632-07-2 ]
YieldReaction ConditionsOperation in experiment
76% at 90℃; for 9h;Neat (no solvent); Aldehyde 1 (1 mmol), dihydrothiophen-3(2H)-one-1,1-dioxide 2 (0.134 g, 1 mmol), enaminone 3 (1 mmol) and were triturated together in an agate mortar for 5 minutes. Then the mixture was kept at 90 C for a certain time (monitored by TLC). The result mixture was washed with water and recrystallized from ethanol (95 %) to give pure product 4.
  • 5
  • [ 17115-51-4 ]
  • [ 36646-78-3 ]
  • [ 123-72-8 ]
  • [ 1265632-08-3 ]
YieldReaction ConditionsOperation in experiment
68% at 90℃; for 10h;Neat (no solvent); Aldehyde 1 (1 mmol), dihydrothiophen-3(2H)-one-1,1-dioxide 2 (0.134 g, 1 mmol), enaminone 3 (1 mmol) and were triturated together in an agate mortar for 5 minutes. Then the mixture was kept at 90 C for a certain time (monitored by TLC). The result mixture was washed with water and recrystallized from ethanol (95 %) to give pure product 4.
  • 6
  • [ 17115-51-4 ]
  • [ 36646-78-3 ]
  • [ 1122-91-4 ]
  • [ 1265632-06-1 ]
YieldReaction ConditionsOperation in experiment
81% at 90℃; for 9h;Neat (no solvent); Aldehyde 1 (1 mmol), dihydrothiophen-3(2H)-one-1,1-dioxide 2 (0.134 g, 1 mmol), enaminone 3 (1 mmol) and were triturated together in an agate mortar for 5 minutes. Then the mixture was kept at 90 C for a certain time (monitored by TLC). The result mixture was washed with water and recrystallized from ethanol (95 %) to give pure product 4.
  • 7
  • [ 17115-51-4 ]
  • [ 36646-78-3 ]
  • [ 456-48-4 ]
  • [ 1265632-04-9 ]
YieldReaction ConditionsOperation in experiment
86% at 90℃; for 9h;Neat (no solvent); Aldehyde 1 (1 mmol), dihydrothiophen-3(2H)-one-1,1-dioxide 2 (0.134 g, 1 mmol), enaminone 3 (1 mmol) and were triturated together in an agate mortar for 5 minutes. Then the mixture was kept at 90 C for a certain time (monitored by TLC). The result mixture was washed with water and recrystallized from ethanol (95 %) to give pure product 4.
 

Historical Records

Technical Information

Categories