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Chemical Structure| 622-33-3 Chemical Structure| 622-33-3
Chemical Structure| 622-33-3

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Product Details of O-Benzylhydroxylamine

CAS No. :622-33-3
Formula : C7H9NO
M.W : 123.15
SMILES Code : NOCC1=CC=CC=C1
MDL No. :MFCD00221709
InChI Key :XYEOALKITRFCJJ-UHFFFAOYSA-N
Pubchem ID :102313

Safety of O-Benzylhydroxylamine

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H301-H314-H335-H412
Precautionary Statements:P261-P264-P270-P271-P273-P280-P301+P310+P330-P301+P330+P331-P303+P361+P353-P304+P340+P310-P305+P351+P338+P310-P363-P403+P233-P405-P501
Class:8
UN#:2735
Packing Group:

Application In Synthesis of O-Benzylhydroxylamine

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 622-33-3 ]

[ 622-33-3 ] Synthesis Path-Downstream   1~5

  • 1
  • [ 622-33-3 ]
  • [ 6645-46-1 ]
  • ((R)-3-Benzyloxycarbamoyl-2-hydroxy-propyl)-trimethyl-ammonium; chloride [ No CAS ]
  • 2
  • [ 109-72-8 ]
  • [ 1293-65-8 ]
  • [ 622-33-3 ]
  • [ 206274-95-5 ]
  • [ 206274-98-8 ]
  • [ 206275-00-5 ]
  • 3
  • [ 622-33-3 ]
  • [ 68-04-2 ]
  • C27H29N3O7 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With pyridine; hydrogenchloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In water; at 20℃; for 1h;pH 5; General procedure: Pyridine buffer was prepared by combining 5.4 ml of HCl(12.1 M), 8.6 ml of pyridine, and 86 ml of water. The pH was measured with pH paper to be around 5.0. Using a Biomek FX workstation(Beckman Coulter, Brea, CA, USA), reconstituted standard curves (in water, in cell matrix, and in tumor matrix) and samples were mixed with 50 ll of 1M O-BHA and 50 ll of 1 M EDC in the pyridine buffer. After 1 h at room temperature, ethyl acetate(300 ll) was added and the plates were shaken for 10 min using a VWR Multi-Tube Vortexer. The organic layer was taken into a96-well 2-ml plate using a Biomek FX workstation. Then the aqueous layer was extracted again with 300 ll of ethyl acetate using theVortexer and Biomek FX workstation. The organic layers were combined into a 96-well 2-ml plate. The 2-ml plate was dried usinga stream of nitrogen at 40 C and reconstituted in 1 ml of 50%methanol/water. The samples were analyzed by LC-MS/MS.
  • 4
  • [ 622-33-3 ]
  • [ 95652-77-0 ]
  • methyl 2-((benzyloxy)amino)-6-methoxynicotinate [ No CAS ]
  • 5
  • [ 622-33-3 ]
  • [ 34374-88-4 ]
  • tris(N-salicylidene(O-benzylhydroxylamine)) [ No CAS ]
 

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