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Chemical Structure| 960492-73-3 Chemical Structure| 960492-73-3

Structure of 960492-73-3

Chemical Structure| 960492-73-3

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3-(2-Bromophenoxy)azetidine hydrochloride

CAS No.: 960492-73-3

,95%

4.5 *For Research Use Only !

Cat. No.: A2280866 Purity: 95%

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    Product Details of [ 960492-73-3 ]

    CAS No. :960492-73-3
    Formula : C9H11BrClNO
    M.W : 264.55
    SMILES Code : BrC1=CC=CC=C1OC2CNC2.[H]Cl
    MDL No. :MFCD17171118

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    Application In Synthesis of [ 960492-73-3 ]

    * All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

    • Downstream synthetic route of [ 960492-73-3 ]

    [ 960492-73-3 ] Synthesis Path-Downstream   1~1

    • 1
    • [ 960492-73-3 ]
    • [ 65202-50-8 ]
    • methyl 6-{3-[(2-bromophenyl)oxy]azetidin-1-yl}pyridazine-3-carboxylate [ No CAS ]
    YieldReaction ConditionsOperation in experiment
    With potassium carbonate; In 1,4-dioxane; for 16h;Heating / reflux; Methyl 6-{3-r(2-bromophenyl)oxylazetidin-l-yl}pyridazine-3-carboxylate; Into a flame-dried 100 mL round-bottom flask equipped with a magnetic stirring bar and under N2 was added <strong>[65202-50-8]methyl 6-chloropyridazine-3-carboxylate</strong> (848 mg, 4.91 mmol), 3- [(2-bromophenyl)oxy]azetidine hydrochloride (1.3 g, 4.91 mmol) and potassium carbonate (2.04 g, 14.7 mmol) in dioxane (30 mL). The reaction mixture was heated to reflux for 16 h overnight. The reaction mixture was cooled to room temperature and quenched with water (10 mL). The reaction mixture was concentrated and a beige solid precipitated out of solution. The solid was diluted with water (20 mL) and filtered through WhatmanNo.l paper on a Hirsch funnel, washing with water. The resulting beige solid was dried on the vacuum pump overnight, giving the desired product.MS (ESI, Q+) m/z 364 (M + 1, 79Br), 366 (M + 1, 81Br).
     

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