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Chemical Structure| 911825-94-0 Chemical Structure| 911825-94-0

Structure of 911825-94-0

Chemical Structure| 911825-94-0

(2-Fluoro-6-iodophenyl)methanol

CAS No.: 911825-94-0

4.5 *For Research Use Only !

Cat. No.: A626285 Purity: 95%

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Product Details of [ 911825-94-0 ]

CAS No. :911825-94-0
Formula : C7H6FIO
M.W : 252.03
SMILES Code : OCC1=C(I)C=CC=C1F
MDL No. :MFCD09910144
InChI Key :ZMLMVTDRUORFDB-UHFFFAOYSA-N
Pubchem ID :59705003

Safety of [ 911825-94-0 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H320-H335
Precautionary Statements:P264-P270-P301+P312-P330

Application In Synthesis of [ 911825-94-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 911825-94-0 ]

[ 911825-94-0 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 111771-08-5 ]
  • [ 911825-94-0 ]
YieldReaction ConditionsOperation in experiment
(2-Fluoro-6-iodophenyl)methanol.; To a stirred solution of <strong>[111771-08-5]2-fluoro-6-iodobenzoic acid</strong> (10 mmol) in THF (6.5 mL) and trimethylborate (3.25 mL) was added borane dimethylsulfide (12 mmol) slowly, maintaining the internal temperature at 20-25 C. Stirring was continued for an additional 16 h at room temperature and then methanol (1.44 mL) was added cautiously. The resulted solution was evaporated in vacuo to offer 2.5 g of the title compound as a pale yellow oil.
With Trimethyl borate; dimethylsulfide borane complex; In tetrahydrofuran; at 20 - 25℃; for 16h; (2-Fluoro-6-iodophenyl)methanoI. To a stirred solution of 2-fluoro-6- iodobenzoic acid (lOmmol) in THF (6.5mL) and trimethylborate (3.25mL) was added borane dimethylsulfide (12mmol) slowly, maintaining the internal temperature at 20- 25 0C. Stirring was continued for an additional 16 h at room temperature and then methanol (1.44mL) was added cautiously. The resulted solution was evaporated in vacuo to offer 2.5 g of the title compound as a pale yellow oil.
 

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