889-31-6|3-(Benzylamino)-5,5-dimethylcyclohex-2-enone| Ambeed

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Quality Control of [ 889-31-6 ] Purity: 95% SDS Specification

COA

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NMR

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CNMR

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Product Details of [ 889-31-6 ]

CAS No. :	889-31-6
Formula :	C₁₅H₁₉NO
M.W :	229.32
SMILES Code :	CC(C1)(C)CC(NCC2=CC=CC=C2)=CC1=O
MDL No. :	MFCD00170309

Safety of [ 889-31-6 ]

GHS Pictogram:
Signal Word:	Warning
Hazard Statements:	H315-H319
Precautionary Statements:	P264-P280-P302+P352-P305+P351+P338-P332+P313-P337+P313-P362

Application In Synthesis of [ 889-31-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 889-31-6 ]

[ 889-31-6 ] Synthesis Path-Downstream 1~9

1
[ 17115-51-4 ]
[ 889-31-6 ]
[ 104-88-1 ]
[ 1265632-12-9 ]

Yield	Reaction Conditions	Operation in experiment
46%	at 90℃; for 15h;Neat (no solvent);	Aldehyde 1 (1 mmol), dihydrothiophen-3(2H)-one-1,1-dioxide 2 (0.134 g, 1 mmol), enaminone 3 (1 mmol) and were triturated together in an agate mortar for 5 minutes. Then the mixture was kept at 90 C for a certain time (monitored by TLC). The result mixture was washed with water and recrystallized from ethanol (95 %) to give pure product 4.

References: [1]Bioorganic and Medicinal Chemistry Letters,2011,vol. 21,p. 453 - 455.

2
[ 17115-51-4 ]
[ 889-31-6 ]
[ 1122-91-4 ]
[ 1265632-13-0 ]

Yield	Reaction Conditions	Operation in experiment
52%	at 90℃; for 14h;Neat (no solvent);	Aldehyde 1 (1 mmol), dihydrothiophen-3(2H)-one-1,1-dioxide 2 (0.134 g, 1 mmol), enaminone 3 (1 mmol) and were triturated together in an agate mortar for 5 minutes. Then the mixture was kept at 90 C for a certain time (monitored by TLC). The result mixture was washed with water and recrystallized from ethanol (95 %) to give pure product 4.

References: [1]Bioorganic and Medicinal Chemistry Letters,2011,vol. 21,p. 453 - 455.

3
[ 889-31-6 ]
[ 762-42-5 ]
[ 100-46-9 ]
[ 873-95-0 ]
[ 73549-66-3 ]