Home Cart Sign in  
Chemical Structure| 80352-66-5 Chemical Structure| 80352-66-5

Structure of 80352-66-5

Chemical Structure| 80352-66-5

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 80352-66-5 ]

CAS No. :80352-66-5
Formula : C6H12O3S
M.W : 164.22
SMILES Code : CS(=O)(OCCC(C)=C)=O
MDL No. :MFCD27500702

Safety of [ 80352-66-5 ]

Application In Synthesis of [ 80352-66-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 80352-66-5 ]

[ 80352-66-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 14381-51-2 ]
  • [ 80352-66-5 ]
  • 3-Bromo-2-((3-methylbut-3-en-1-yl)oxy)phenol [ No CAS ]
  • 6-Bromo-2-((3-methylbut-3-en-1-yl)oxy)phenol [ No CAS ]
YieldReaction ConditionsOperation in experiment
[00220] A mixture of compound 1-3 (3.0 g, 15.87 mmol), compound 91- 2 (2.6 g, 15.87 mmol), potassium carbonate (2.2 g, 15.87 mmol) and potassium iodide (266 mg, 1.6 mmol) in DMF (50 ml) was stirred at 60°C overnight. After concentration, the residue was dissolved in water (25 ml) and acidified with 6 N hydrochloric acid to pH = 2. The mixture was extracted with dichloromethane (20 ml chi 3), and the combined dichloromethane was washed with water and brine, dried over anhydrous Na2S04. The solvent was removed under vacuum and the crude product was purified by flash chromatography on silica gel (petroleum ether/ethyl acetate = 50:1) to give I .48 g of the mixture of compound 91-3 and 91-3B as colorless oil (yield 36percent). [00221] 1H NMR deltaEta (400 MHz; CDCI3): 1.80-1.84 (m, 3H), 2.49-2.54 (m, 2H), 4.10-4.22 (m, 2H), 4.82-5.00 (m, 2H), 6.03-6.07 (m, 1 H), 6.72-6.88 (m, 2H), 7.02-7.11 (m, 1 H).
 

Historical Records