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Chemical Structure| 69506-86-1 Chemical Structure| 69506-86-1

Structure of 69506-86-1

Chemical Structure| 69506-86-1

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Product Details of [ 69506-86-1 ]

CAS No. :69506-86-1
Formula : C10H14N4
M.W : 190.25
SMILES Code : N1(CCCCN2C=CN=C2)C=CN=C1
MDL No. :MFCD00608317
InChI Key :LGCPYQSYWVJQCJ-UHFFFAOYSA-N
Pubchem ID :5251826

Safety of [ 69506-86-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis of [ 69506-86-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 69506-86-1 ]

[ 69506-86-1 ] Synthesis Path-Downstream   1~8

  • 1
  • [ 69506-86-1 ]
  • copper(II) acetate tetrahydrate [ No CAS ]
  • [ 499-49-0 ]
  • [Cu2(5-methyl isophthalate)2(1,1'-(1,4-butanediyl)bis(imidazole))] [ No CAS ]
  • 2
  • [ 69506-86-1 ]
  • [ 162709-84-4 ]
  • 1,1'-(1,4-butanediyl)bis{3-[3,4,5-tris(dodecyloxy)benzyl]imidazolium} dichloride [ No CAS ]
  • 3
  • [ 69506-86-1 ]
  • [ 23351-91-9 ]
  • [ 6018-89-9 ]
  • [ 1314760-62-7 ]
  • 4
  • [ 69506-86-1 ]
  • [ 499-49-0 ]
  • [ 6147-53-1 ]
  • [Co(5-methylisophthalate)(1,4-bis(imidazol-1-yl)butane)]·2H2O}n [ No CAS ]
  • 5
  • [ 69506-86-1 ]
  • dodecamolybdophosphoric acid * 13 H2O [ No CAS ]
  • [ 69506-85-0 ]
  • [(PMo12O40)(1,1 '-(1,4-butanediyl)bis(imidazole)(+2H))0.5(1,1'-(1,3-propanediyl)bis(imidazole)(+H))] [ No CAS ]
YieldReaction ConditionsOperation in experiment
63% With hydrogenchloride; In water; at 25 - 170℃; for 96h;pH 4.0;Autoclave; A mixture of H3PMo12O40·13H2O (0.6178g, 0.3mmol), bpi (0.0175g, 0.1mmol), bbi (0.019g, 0.1mmol) and H2O (10ml) was stirred for 30min in air until it was homogeneous. When the pH value of the mixture was adjusted to 4 with 1M HCl, the solution was transferred and sealed in a 30-ml Teflon-lined stainless steel autoclave, which was heated at 170C under autogenous pressure for 4days. The light blue sheet crystals were isolated and collected by filtration, washed thoroughly with distilled water, and dried at room temperature (63% yield based on Mo). Anal. Calc. C14H21N6O40PMo12 (2095.62): C, 7.99 (Calc. 8.02); H, 0.99 (1.00); N, 3.99 (4.01); P, 1.44 (1.48); Mo, 54.61 (54.97) wt.%.
  • 6
  • [ 69506-86-1 ]
  • [ 499-49-0 ]
  • [ 7732-18-5 ]
  • [ 5743-04-4 ]
  • [cadmium(II)(1,4-bis(imidazole)butane)(5-methylisophthalate)(H2O)]*H2O}2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
45% With potassium hydroxide; In water; at 139.84℃; for 72h;Autoclave; The reaction condition is similar to those described in 1 except that 1,2-bie was replaced by 1,4-bib (19.0mg, 0.1mmol). Colorless block crystals of 3 were obtained. Yield: 23.3mg, 45percent (Based on Cd). Anal. Calc. for C38H48Cd2N8O12: C, 44.16; H, 4.68; N, 12.84. Found: C, 44.23; H, 4.78; N, 12.77percent. IR (cm?1): 3446 m, 3128 m, 2591 m, 1548 s, 1439 s, 1369 s, 1111 s, 774 s, 730 s, 657 s.
  • 7
  • zinc(II) nitrate hexahydrate [ No CAS ]
  • [ 69506-86-1 ]
  • [ 130-85-8 ]
  • Zn(2+)*C10H14N4*C23H14O6(2-) [ No CAS ]
YieldReaction ConditionsOperation in experiment
35% In water; N,N-dimethyl-formamide; at 120℃; for 60h;Autoclave; A mixture of Zn(NO3)2.6H2O (0.030 g, 0.10 mmol), H2pam (0.030 g,0.10 mmol), bib (0.019 g, 0.1 mmol), DMF (2 mL), andH2O (2 mL) was placed in a Parr Teflon-lined stainless steelvessel (23 mL). Then the vessel was sealed and heated to120C, and hold for 60 h. Then the reactant mixture wascooled to room temperature at a rate of 0.5C/min, leadingto the formation of crystal 1in 35percent yield based on Zn(II).Anal. Calcd. for C33H25N4O6Zn (637.95): C, 62.07; N, 8.78;H, 3.76percent. Found: C, 62.08; N, 8.76; H, 3.79percent.
  • 8
  • [ 69506-86-1 ]
  • [ 16427-44-4 ]
  • C16H28N4O2(2+)*2CH3O3S(1-) [ No CAS ]
YieldReaction ConditionsOperation in experiment
at 70℃; for 24h; 0.02 mol of 1,4-bisimidazolidine and 0.04 mol of <strong>[16427-44-4]ethylene glycol methyl ether methyl sulfonate</strong> added to the drying tube,Thermometer and equipped with a rotor in a three-necked flask,A three-necked flask was placed in a collector type thermostatic magnetic stirrer containing a heat transfer oil,The oil bath was heated to a temperature of 70 & lt; 0 & gt; C inside the flask,Continuous stirring 24h,After the reaction was completed, a viscous liquid with a yellow band was obtained,The liquid was collected,And dried in a vacuum oven at 80 & lt; 0 & gt; C for 6 h,Thereby obtaining an ether-based bisimidazolium ionic liquid for absorbing SO2Bis- (3-ethylene glycol methyl ether-1-imidazole) butylene dimethanesulfonate,
 

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