Home Cart Sign in  
HazMat Fee +

There will be a HazMat fee per item when shipping a dangerous goods. The HazMat fee will be charged to your UPS/DHL/FedEx collect account or added to the invoice unless the package is shipped via Ground service. Ship by air in Excepted Quantity (each bottle), which is up to 1g/1mL for class 6.1 packing group I or II, and up to 25g/25ml for all other HazMat items.

Type HazMat fee for 500 gram (Estimated)
Excepted Quantity USD 0.00
Limited Quantity USD 15-60
Inaccessible (Haz class 6.1), Domestic USD 80+
Inaccessible (Haz class 6.1), International USD 150+
Accessible (Haz class 3, 4, 5 or 8), Domestic USD 100+
Accessible (Haz class 3, 4, 5 or 8), International USD 200+
Chemical Structure| 68664-23-3 Chemical Structure| 68664-23-3

Structure of 3-Phenylpropyl isocyanate
CAS No.: 68664-23-3

Chemical Structure| 68664-23-3

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 68664-23-3 ]

CAS No. :68664-23-3
Formula : C10H11NO
M.W : 161.20
SMILES Code : O=C=NCCCC1=CC=CC=C1
MDL No. :MFCD04039909

Safety of [ 68664-23-3 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302-H312-H319-H332-H334
Precautionary Statements:P261-P280-P305+P351+P338-P342+P311
Class:6.1
UN#:2206
Packing Group:

Application In Synthesis of [ 68664-23-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 68664-23-3 ]

[ 68664-23-3 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 68664-23-3 ]
  • [ 23357-46-2 ]
  • (R)-1-(3-phenylpropyl)-3-(1,2,3,4-tetrahydronaphthalen-1-yl)urea [ No CAS ]
YieldReaction ConditionsOperation in experiment
81% In acetonitrile; at 20℃; for 8h; General procedure: To the corresponding amine 9 (0.710mmol) in acetonitrile (5mL), 3-phenylpropyl isocyanate 10 (0.645mmol) was added and allowed to stir for 8hat ambient temperature. The resulting mixture was portioned between water and ethyl acetate. The organic layer was dried over anhydrous Na2SO4 and evaporated under reduced pressure. The crude mixture was subjected to column chromatography to obtain the pure compounds. 5.1.1.15 (R)-1-(3-phenylpropyl)-3-(1,2,3,4-tetrahydronaphthalen-1-yl)urea (8h(R)) Yield 81%; White solid; mp 133-135 C; IR (neat): 3315, 2999, 2942, 1621, 1571, 1498, 1450 cm-1; 1H NMR (CDCl3) δ 1.74-1.88 (m, 6H), 1.99-2.04 (m, 1H), 2.65 (t, J = 7.80 Hz, 2H), 2.70-2.81 (m, 2H), 3.19 (t, J = 7.20 Hz, 2H), 4.60-4.75 (bs, 1H), 4.92-4.94 (m, 1H), 7.07-7.31 (m, 9H); 13C NMR (CDCl3) δ 19.92, 29.19, 30.68, 31.44, 33.05, 40.30, 48.89, 126.03, 126.25, 127.28, 128.34, 128.48, 128.61, 129.12, 136.94, 137.50, 141.23, 157.80; HRMS Calcd for C20H24N2O m/z [M+H] 309.1967, found 309.1999.
  • 2
  • [ 68664-23-3 ]
  • [ 1006-64-0 ]
  • (S)-2-phenyl-N-(3-phenylpropyl)pyrrolidine-1-carboxamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
82% In acetonitrile; at 20℃; for 8h; General procedure: To the corresponding amine 9 (0.710mmol) in acetonitrile (5mL), 3-phenylpropyl isocyanate 10 (0.645mmol) was added and allowed to stir for 8hat ambient temperature. The resulting mixture was portioned between water and ethyl acetate. The organic layer was dried over anhydrous Na2SO4 and evaporated under reduced pressure. The crude mixture was subjected to column chromatography to obtain the pure compounds. 5.1.1.16 (S)-2-phenyl-N-(3-phenylpropyl)pyrrolidine-1-carboxamide (8i(S)) Yield 82%; Yellow oil; IR (neat): 3335, 3025, 2864, 1628, 1527, 1494, 1346 cm-1; 1H NMR (CDCl3) delta 1.60-1.67 (m, 2H), 1.82-194 (m, 3H), 2.35-2.42 (m, 3H), 3.04-3.11 (m, 1H), 3.15-3.22 (m, 1H), 3.63-3.72 (m, 2H), 4.01 (bs, 1H), 4.64-4.67 (m, 1H), 7.01 (d, J = 7.60 Hz, 2H), 7.13-7.37 (m, 8H); 13C NMR (CDCl3) delta 23.02, 31.58, 32.84, 36.78, 39.87, 47.27, 60.84, 125.74, 125.78, 127.57, 128.33, 128.34, 128.97, 141.76, 143.33, 157.12; HRMS Calcd for C20H24N2O m/z [M+H] 309.1967, found 309.1996.
  • 3
  • [ 68664-23-3 ]
  • [ 56523-47-8 ]
  • (R)-2-phenyl-N-(3-phenylpropyl)pyrrolidine-1-carboxamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
86% In acetonitrile; at 20℃; for 8h; General procedure: To the corresponding amine 9 (0.710mmol) in acetonitrile (5mL), 3-phenylpropyl isocyanate 10 (0.645mmol) was added and allowed to stir for 8hat ambient temperature. The resulting mixture was portioned between water and ethyl acetate. The organic layer was dried over anhydrous Na2SO4 and evaporated under reduced pressure. The crude mixture was subjected to column chromatography to obtain the pure compounds. 5.1.1.17 (R)-2-phenyl-N-(3-phenylpropyl)pyrrolidine-1-carboxamide (8i(R)) Yield 86%; Yellow oil; IR (neat): 3335, 3025, 2863, 1628, 1528, 1494, 1346 cm-1; 1H NMR (CDCl3) δ 1.60-1.68 (m, 2H), 1.83-1.94 (m, 3H), 2.34-2.43 (m, 3H), 3.03-3.12 (m, 1H), 3.15-3.24 (m, 1H), 3.65-3.72 (m, 2H), 4.64-4.68 (m, 1H), 7.00-7.02 (m, 2H), 7.12-7.29 (m, 6H), 7.33-7.39 (m, 2H). 13C NMR (CDCl3) δ 23.11, 31.58, 32.90, 36.74, 40.10, 47.58, 61.18, 125.76, 127.65, 128.30, 128.31, 128.97, 141.63, 142.85, 156.96; HRMS Calcd for C20H24N2O m/z [M+H] 309.1967, found 309.1995.
  • 4
  • [ 41764-74-3 ]
  • [ 68664-23-3 ]
  • 2-(3,4-dimethoxybenzoyl)-N-(3-phenylpropyl)hydrazine-1-carboxamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
90% In acetonitrile; at 20℃; for 8h; General procedure: To a solution of hydrazide intermediates 10d,k,l,n (1.85 mmol) in acetonitrile, corresponding isocyanates 15a-c was added and stirred for 8 h at ambient temperature. After the formation of product monitored by TLC, water was added and extracted using ethylacetate. The organic layer was dried over anhydrous sodium sulfate and evaporated under vacuum. The crude product was purified using column chromatography to get 16a-f.
 

Historical Records