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Chemical Structure| 66624-36-0 Chemical Structure| 66624-36-0

Structure of 66624-36-0

Chemical Structure| 66624-36-0

(3-Fluoro-4-methoxyphenyl)(methyl)sulfane

CAS No.: 66624-36-0

4.5 *For Research Use Only !

Cat. No.: A962041 Purity: 97%

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Product Details of [ 66624-36-0 ]

CAS No. :66624-36-0
Formula : C8H9FOS
M.W : 172.22
SMILES Code : CSC1=CC=C(OC)C(F)=C1
MDL No. :MFCD11617749

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Application In Synthesis of [ 66624-36-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 66624-36-0 ]

[ 66624-36-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 66624-36-0 ]
  • [ 20951-14-8 ]
YieldReaction ConditionsOperation in experiment
With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20℃; for 2.0h; To a stirred solution of the product from Step B (557 mg, 3.24 mmol) in dichloromethane ( 15 mL) was added m-chloroperbenzoic acid (2.19 g, 12.7 mmol). After stirring at room temperature for 2 h, the reaction was diluted with ethyl acetate. The organic phase was washed sequentially with 1 N aqueous sodium hydroxide solution and brine, and concentrated in vacuo. Purification by flash chromatography (silica gel, 75:25 hexanes/ethyl acetate) afforded the desired compound.
 

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