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Chemical Structure| 65009-00-9 Chemical Structure| 65009-00-9

Structure of 65009-00-9

Chemical Structure| 65009-00-9
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Product Details of [ 65009-00-9 ]

CAS No. :65009-00-9
Formula : C11H15NO2
M.W : 193.24
SMILES Code : O=C(OC1=CC=CC=C1)N(CC)CC
MDL No. :MFCD00594379

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Application In Synthesis of [ 65009-00-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 65009-00-9 ]

[ 65009-00-9 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 109-01-3 ]
  • [ 65009-00-9 ]
  • [ 90-89-1 ]
  • 2
  • [ 1006-68-4 ]
  • [ 65009-00-9 ]
  • [ 92-71-7 ]
YieldReaction ConditionsOperation in experiment
64% With bis(1,5-cyclooctadiene)nickel(0); potassium phosphate; 3,4-thiene-2,3-diylbis(dicyclohexylphosphine); In para-xylene; at 140℃; for 22h;Glovebox; Sealed tube; General procedure: Ni(COD)2, ligand (dcype or dcypt), base (Cs2CO3 or K3PO4), and azole were weighed into in an oven dried 20 mL scintillation vial in the glove box. A xylene solution of the aryl electrophile (pivalates, mesylates or carbamates) was added to the reaction mixture. The reaction vial was sealed with a Teflon lined cap, taken out of the glove box and the reaction mixture was allowed to stir at the indicated temperature for the indicated time. The reaction mixture was cooled to room temperature and filtered through a 1.0 inch plug of silica gel, eluting with Et2O (125 mL). The filtrate was concentrated and chromatographed on a silica gel column to afford the product.
 

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