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CAS No. : | 6499-15-6 | MDL No. : | MFCD00588818 |
Formula : | C5H11N3OS | Boiling Point : | - |
Linear Structure Formula : | O(C2H4)2NC(S)NHNH2 | InChI Key : | - |
M.W : | 161.23 | Pubchem ID : | - |
Synonyms : |
Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
Hazard Statements: | Packing Group: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
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52% | General procedure: Sodium (0.092 g, 4.0 mmol) was added to dried methanol (25 mL), and stirred until complete dissolution was achieved. 2-Cyanopyridine or substituted 2-cyanopyridine (24.9 mmol) was then added. The mixture was stirred for 30 min. The N(4)-disubstituted thiosemicarbazide (24.9 mmol) was then added in small portions over a period of 1 h. A further quantity of methanol (25 mL) was added and the mixture was heated under reflux for a minimum of 4 h. Slow evaporation of the methanol produced the crystals of the desired product.(See Supplementary data) |