Home Cart Sign in  
Chemical Structure| 6240-00-2 Chemical Structure| 6240-00-2

Structure of 6240-00-2

Chemical Structure| 6240-00-2

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 6240-00-2 ]

CAS No. :6240-00-2
Formula : C13H19NO3
M.W : 237.30
SMILES Code : O=C(C12CC3(NC(C)=O)CC(C2)CC(C3)C1)O
MDL No. :MFCD00154633

Safety of [ 6240-00-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P362-P403+P233-P501

Application In Synthesis of [ 6240-00-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 6240-00-2 ]

[ 6240-00-2 ] Synthesis Path-Downstream   1~2

  • 2
  • [ 6240-00-2 ]
  • [ 6240-01-3 ]
YieldReaction ConditionsOperation in experiment
78% With hydrogenchloride; water; at 95℃; for 144.0h; Step 2: 3-Amino-adamantane-1-carboxylic acid hydrochloride; To a 3-neck 5-L flask equipped with a reflux condenser, a mechanical stirrer and a temperature probe was added 3-acetylamino-adamantane-1-carboxylic acid (432 g, 1.82 mol), water (1.00 L) and concentrated hydrochloric acid (2.44 L), and the resulting mixture was heated at 95 C. for 6 days. During this time, solid material precipitated from the solution. After cooling at 0 C., the solids were filtered and washed with acetone. The solid was then dried under high vacuum at 50 C. for about 2 hours to afford 328 g (78%) of the title compound, 3-amino-adamantane-1-carboxylic acid hydrochloride, as a white solid. 1H NMR (300 MHz, DMSO-td6) delta 12.35 (br s, 1H), 8.27 (br s, 3H), 2.22-2.12 (m, 2H), 1.92-1.85 (m, 2H), 1.83-1.71 (ml 6H), 1.69-1.48 (m, 4H).
 

Historical Records

Technical Information

Categories