Home Cart Sign in  
Chemical Structure| 62368-29-0 Chemical Structure| 62368-29-0

Structure of 62368-29-0

Chemical Structure| 62368-29-0

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 62368-29-0 ]

CAS No. :62368-29-0
Formula : C10H12N2O
M.W : 176.22
SMILES Code : NC1=CC2=C(C=C1)CCN2C(C)=O
MDL No. :MFCD00056021

Safety of [ 62368-29-0 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H319
Precautionary Statements:P305+P351+P338

Application In Synthesis of [ 62368-29-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 62368-29-0 ]

[ 62368-29-0 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 22949-08-2 ]
  • [ 62368-29-0 ]
YieldReaction ConditionsOperation in experiment
99% With hydrogen;palladium 10% on activated carbon; In ethyl acetate; under 2068.65 - 2844.39 Torr; for 2.0h; Step B: l-Acetyl-6-nitroindoline (3.8 g, 18.3 mmol) was suspended in EtOAc (200 mL). Pd/C (650 mg, 10%) was added, and the mixture was hydrogenated at 40-55 p.si.i. for 2 hours. The mixture was then filtered through celite. The filtrate was concentrated, and the residue was triturated with ether to yield l-acetyl-6-aminoindoline (3.18 g, 99%) as an orange solid.
  • 2
  • [ 62368-29-0 ]
  • [ 24686-78-0 ]
  • 1-[6-(1-Benzoyl-piperidin-4-ylamino)-2,3-dihydro-indol-1-yl]-ethanone [ No CAS ]
YieldReaction ConditionsOperation in experiment
30% With sodium tris(acetoxy)borohydride; acetic acid; In dichloromethane; To a solution of 1 -benzoyl-4-piperidone (250 mg, 1.2 mmol) and 1-acetyl-6-aminoindoline (220 mg, 1.2 mmol), in CH2Cl2 (0.2 M) was added AcOH (73 muL, 1.2 mmol), followed by Na(OAc)3BH (390 mg, 1.8 mmol). The resulting solution was allowed to stir overnight. The reaction was quenched by the addition of satd. aq. NaHCO3 and CH2Cl2. The layers were separated, and the organic portion was washed with brine, dried with Na2SO4 and concentrated. Purification by silica gel chromatography (1 to 5percent MeOH/CH2Cl2) provided the desired intermediate (132 mg, 30percent).
 

Historical Records

Technical Information

Categories