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Chemical Structure| 614731-22-5 Chemical Structure| 614731-22-5

Structure of 614731-22-5

Chemical Structure| 614731-22-5

4-((2-Fluorophenoxy)methyl)piperidine hydrochloride

CAS No.: 614731-22-5

4.5 *For Research Use Only !

Cat. No.: A259519 Purity: 95%

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Product Details of [ 614731-22-5 ]

CAS No. :614731-22-5
Formula : C12H17ClFNO
M.W : 245.72
SMILES Code : FC1=CC=CC=C1OCC2CCNCC2.[H]Cl
MDL No. :MFCD08445758

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Application In Synthesis of [ 614731-22-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 614731-22-5 ]

[ 614731-22-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 614731-22-5 ]
  • [ 252742-72-6 ]
  • [ 614729-03-2 ]
YieldReaction ConditionsOperation in experiment
21% With potassium carbonate; In water; ethyl acetate; acetonitrile; Example 405 5-(4-(2-Fluorophenoxymethyl)piperidino]methyl-2,4-dihydro-[1,2,4]triazol-3-one After adding 150 mg of <strong>[252742-72-6]5-chloromethyl-2,4-dihydro-[1,2,4]triazol-3-one</strong>, 331 mg of 4-(2-fluorophenoxymethyl)piperidine hydrochloride and 180 mg of anhydrous potassium carbonate to acetonitrile, the mixture was stirred overnight at room temperature. Water and ethyl acetate were added to the reaction mixture and the insoluble portion was filtered out to obtain the title compound (70 mg, 21percent yield). 1H-NMR (400 MHz, DMSO-d6); delta (ppm) 1.26-1.38 (2H, m), 1.67-1.80 (3H, m), 1.95-2.04 (2H, m), 2.77-2.84 (2H, m), 3.24 (2H, s), 3.88 (2H, d, J=5.6 Hz), 6.87-6.94 (1H, m), 7.06-7.21 (3H, m), 11.19 (1H, s), 11.27 (1H, br s).
 

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