59969-65-2|(2S,3R)-3-(((Benzyloxy)carbonyl)amino)-2-hydroxy-4-phenylbutanoic acid| Ambeed

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Quality Control of [ 59969-65-2 ] Purity: 95% SDS Specification

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Product Details of [ 59969-65-2 ]

CAS No. :	59969-65-2
Formula :	C₁₈H₁₉NO₅
M.W :	329.35
SMILES Code :	O=C(O)[C@@H](O)[C@H](NC(OCC1=CC=CC=C1)=O)CC2=CC=CC=C2
MDL No. :	MFCD23701663
InChI Key :	JXJYTERRLRAUSF-CVEARBPZSA-N
Pubchem ID :	11067450

Safety of [ 59969-65-2 ]

GHS Pictogram:
Signal Word:	Warning
Hazard Statements:	H302-H315-H319-H335
Precautionary Statements:	P261-P305+P351+P338

Application In Synthesis of [ 59969-65-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 59969-65-2 ]

[ 59969-65-2 ] Synthesis Path-Downstream 1~35

1
[ 2666-93-5 ]
[ 59969-65-2 ]
(2S,3R)-AHPA-(S)-Leu-OMe [ No CAS ]

References: [1]Patent: FR2318863,1977,B1 .
Chem.Abstr.,1977,vol. 87.
Chem.Abstr.,1977,vol. 87.

2
[ 1738-69-8 ]
[ 59969-65-2 ]
[ 60016-66-2 ]

References: [1]Patent: FR2318863,1977,B1 .
Chem.Abstr.,1977,vol. 87.
Chem.Abstr.,1977,vol. 87.

3
[ 2768-50-5 ]
[ 59969-65-2 ]
Z-(2S,3R)-AHPA-(S)-Val(OBzl)-OBzl [ No CAS ]

References: [1]Patent: FR2318863,1977,B1 .
Chem.Abstr.,1977,vol. 87.
Chem.Abstr.,1977,vol. 87.

4
[ 21760-98-5 ]
[ 59969-65-2 ]
Z-(2S,3R)-AHPA-(S)-Val-OBzl [ No CAS ]

References: [1]Patent: FR2318863,1977,B1 .
Chem.Abstr.,1977,vol. 87.
Chem.Abstr.,1977,vol. 87.

5
L-isoleucine benzyl ester [ No CAS ]
[ 59969-65-2 ]
Z-(2S,3R)-AHPA-(S)-Ile-OBzl [ No CAS ]

References: [1]Patent: FR2318863,1977,B1 .
Chem.Abstr.,1977,vol. 87.
Chem.Abstr.,1977,vol. 87.

6
[ 962-39-0 ]
[ 59969-65-2 ]
Z-(2S,3R)-AHPA-(S)-Phe-OBzl [ No CAS ]

References: [1]Patent: FR2318863,1977,B1 .
Chem.Abstr.,1977,vol. 87.
Chem.Abstr.,1977,vol. 87.

7
[ 56145-90-5 ]
[ 59969-65-2 ]
Z-(2S,3R)-AHPA-(S)-Nva-OBzl [ No CAS ]

References: [1]Patent: FR2318863,1977,B1 .
Chem.Abstr.,1977,vol. 87.
Chem.Abstr.,1977,vol. 87.

8
[ 63219-54-5 ]
[ 59969-65-2 ]
Z-(2S,3R)-AHPA-(S)-Nle-OBzl [ No CAS ]

References: [1]Patent: FR2318863,1977,B1 .
Chem.Abstr.,1977,vol. 87.
Chem.Abstr.,1977,vol. 87.

9
[ 63219-55-6 ]
[ 59969-65-2 ]
Z-(2S,3R)-AHPA-(S)-Nle-OBzl [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1977,vol. 20,p. 510 - 515.

10
[ 42854-62-6 ]
[ 59969-65-2 ]
(S)-2-((2S,3R)-3-Benzyloxycarbonylamino-2-hydroxy-4-phenyl-butyrylamino)-propionic acid benzyl ester [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1977,vol. 20,p. 510 - 515.

11
[ 1738-77-8 ]
[ 59969-65-2 ]
[ 60016-66-2 ]

References: [1]Tetrahedron Letters,1984,vol. 25,p. 5079 - 5082.
[2]Journal of Medicinal Chemistry,1977,vol. 20,p. 510 - 515.
[3]Bioscience, Biotechnology and Biochemistry,1999,vol. 63,p. 1304 - 1307.

12
[ 46741-65-5 ]
[ 59969-65-2 ]
[ 62058-27-9 ]

References: [1]Patent: FR2318863,1977,B1 .
Chem.Abstr.,1977,vol. 87.
Chem.Abstr.,1977,vol. 87.

13
[ 59969-65-2 ]
[ 1738-76-7 ]
[ 62023-09-0 ]

References: [1]Journal of Medicinal Chemistry,1977,vol. 20,p. 510 - 515.

14
[ 59969-65-2 ]
[ 16652-76-9 ]
Z-(2S,3R)-AHPA-(S)-Val-OBzl [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1977,vol. 20,p. 510 - 515.

15
[ 59969-65-2 ]
[ 1738-78-9 ]
Z-(2S,3R)-AHPA-(S)-Phe-OBzl [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1977,vol. 20,p. 510 - 515.

16
[ 59969-65-2 ]
[ 16652-75-8 ]
(2S,3S)-2-((2S,3R)-3-Benzyloxycarbonylamino-2-hydroxy-4-phenyl-butyrylamino)-3-methyl-pentanoic acid benzyl ester [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1977,vol. 20,p. 510 - 515.

17
[ 59969-65-2 ]
[ 27019-47-2 ]
[ 62023-41-0 ]

References: [1]Journal of Medicinal Chemistry,1977,vol. 20,p. 510 - 515.

18
[ 59969-65-2 ]
[ 2791-84-6 ]
Z-(2S,3R)-AHPA-(S)-Val(OBzl)-OBzl [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1977,vol. 20,p. 510 - 515.

19
[ 59969-65-2 ]
2-Amino-octanoic acid benzyl ester [ No CAS ]
Z-(2S,3R)-AHPA-(R,S)-Aoc-OBzl [ No CAS ]

References: [1]Patent: FR2318863,1977,B1 .
Chem.Abstr.,1977,vol. 87.
Chem.Abstr.,1977,vol. 87.

20
[ 59969-65-2 ]
[ 26727-22-0 ]
4-((2S,3R)-3-Amino-2-hydroxy-4-phenyl-butyrylamino)-butyric acid [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1977,vol. 20,p. 510 - 515.

21
[ 59969-65-2 ]
[ 5514-99-8 ]
6-((2S,3R)-3-Benzyloxycarbonylamino-2-hydroxy-4-phenyl-butyrylamino)-hexanoic acid benzyl ester [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1977,vol. 20,p. 510 - 515.

22
[ 59969-65-2 ]
[ 63219-58-9 ]
Z-(2S,3R)-AHPA-(R,S)-Aoc-OBzl [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1977,vol. 20,p. 510 - 515.

23
[ 59969-65-2 ]
[ 17664-93-6 ]
[ 62058-27-9 ]

References: [1]Journal of Medicinal Chemistry,1977,vol. 20,p. 510 - 515.

24
[ 59969-65-2 ]
[ 66449-94-3 ]
Z-(2S,3R)-AHPA-(S)-Glu-OBzl [ No CAS ]

References: [1]Patent: FR2318863,1977,B1 .
Chem.Abstr.,1977,vol. 87.
Chem.Abstr.,1977,vol. 87.

25
[ 59969-65-2 ]
[ 16964-83-3 ]
(S)-6-Benzyloxycarbonylamino-2-((2S,3R)-3-benzyloxycarbonylamino-2-hydroxy-4-phenyl-butyrylamino)-hexanoic acid benzyl ester [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1977,vol. 20,p. 510 - 515.

26
[ 59969-65-2 ]
[ 87329-50-8 ]
Z-(2S,3R)-AHPA-(S)-Glu-OBzl [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1977,vol. 20,p. 510 - 515.

27
[ 59969-65-2 ]
(S)-2-Amino-3-benzyloxy-propionic acid 4-nitro-benzyl ester [ No CAS ]
Z-(2S,3R)-AHPA-(S)-Ser(OBzl)-ONb [ No CAS ]

References: [1]Patent: FR2318863,1977,B1 .
Chem.Abstr.,1977,vol. 87.
Chem.Abstr.,1977,vol. 87.

28
[ 59969-65-2 ]
norvaline benzyl ester toluenesulfonate salt [ No CAS ]
Z-(2S,3R)-AHPA-(S)-Nva-OBzl [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1977,vol. 20,p. 510 - 515.

29
[ 59969-65-2 ]
(S)-2-Amino-3-(4-nitro-benzyloxy)-propionic acid benzyl ester; compound with toluene-4-sulfonic acid [ No CAS ]
(S)-2-((2S,3R)-3-Benzyloxycarbonylamino-2-hydroxy-4-phenyl-butyrylamino)-3-(4-nitro-benzyloxy)-propionic acid benzyl ester [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1977,vol. 20,p. 510 - 515.

30
[ 59969-65-2 ]
[ 59554-14-2 ]

References: [1]Journal of Medicinal Chemistry,1977,vol. 20,p. 510 - 515.

31
[ 151-50-8 ]
[ 501-53-1 ]
[ 62023-23-8 ]
[ 59969-65-2 ]

References: [1]Journal of Medicinal Chemistry,1977,vol. 20,p. 510 - 515.

32
[ 908094-01-9 ]
[ 59969-65-2 ]
[ 124782-04-3 ]

References: [1]Tetrahedron Letters,1993,vol. 34,p. 5127 - 5130.
[2]Heterocycles,1996,vol. 42,p. 701 - 722.

33
[ 124782-04-3 ]
[ 59969-65-2 ]

References: [1]Journal of Organic Chemistry,1990,vol. 55,p. 2232 - 2234.
[2]Synthesis,1989,p. 703 - 706.

34
[ 59554-14-2 ]
[ 501-53-1 ]
[ 59969-65-2 ]

Yield	Reaction Conditions	Operation in experiment
64%	With sodium hydroxide; In tetrahydrofuran; at 20℃; for 6h;Cooling with ice;	AHPA(1,1.95g, 10.0mmol)Dissolved in a mixed solution of 100 mL of tetrahydrofuran and 1 mol/L of sodium hydroxide,Benzyloxycarbonyl chloride (1.88 g, 11.0 mmol) was added dropwise under ice bath.After reacting at room temperature for 6 hours, the tetrahydrofuran in the reaction solution was distilled off.The aqueous phase was adjusted to pH 1 with 1 mol/L hydrochloric acid, and extracted with ethyl acetate three times.The organic phases were combined and dried over anhydrous magnesium sulfate.Evaporation of the solvent to give a white solid 2(2.11g, 64%).

References: [1]Patent: CN109053782,2018,A .Location in patent: Paragraph 0017; 0067; 0068.
[2]Tetrahedron Letters,1984,vol. 25,p. 5079 - 5082.

35
[ 152897-53-5 ]
[ 59969-65-2 ]

References: [1]Tetrahedron Letters,1993,vol. 34,p. 5127 - 5130.
[2]Heterocycles,1996,vol. 42,p. 701 - 722.

Historical Records

Technical Information

• Arndt-Eistert Homologation • Hunsdiecker-Borodin Reaction • Passerini Reaction • Preparation of Amines • Preparation of Carboxylic Acids • Reactions of Amines • Reactions of Benzene and Substituted Benzenes • Reactions of Carboxylic Acids • Schmidt Reaction • Specialized Acylation Reagents-Ketenes • Ugi Reaction

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P342	If experiencing respiratory symptoms:
P350	Gently wash with plenty of soap and water.
P351	Rinse cautiously with water for several minutes.
P352	Wash with plenty of soap and water.
P353	Rinse skin with water/shower.
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P362	Take off contaminated clothing and wash before reuse.
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P370	In case of fire:
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P377	Leaking gas fire: Do not extinguish, unless leak can be stopped safely.
P378
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P390	Absorb spillage to prevent material damage.
P391	Collect spillage. Hazardous to the aquatic environment
P301 + P310	IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.
P301 + P312	IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P301 + P330 + P331	IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P302 + P334	IF ON SKIN: Immerse in cool water/wrap in wet bandages.
P302 + P350	IF ON SKIN: Gently wash with plenty of soap and water.
P303 + P361 + P353	IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P304 + P312	IF INHALED: Call a POISON CENTER or doctor/physician if you feel unwell.
P304 + P340	IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P304 + P341	IF INHALED: If breathing is difficult, remove victim to fresh air and keep at rest in a position comfortable for breathing.
P305 + P351 + P338	IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P306 + P360	IF ON CLOTHING: Rinse Immediately contaminated CLOTHING and SKIN with plenty of water before removing clothes.
P307 + P311	IF exposed: call a POISON CENTER or doctor/physician.
P308 + P313	IF exposed or concerned: Get medical advice/attention.
P309 + P311	IF exposed or if you feel unwell: call a POISON CENTER or doctor/physician.
P332 + P313	IF SKIN irritation occurs: Get medical advice/attention.
P333 + P313	IF SKIN irritation or rash occurs: Get medical advice/attention.
P335 + P334	Brush off loose particles from skin. Immerse in cool water/wrap in wet bandages.
P337 + P313	IF eye irritation persists: Get medical advice/attention.
P342 + P311	IF experiencing respiratory symptoms: call a POISON CENTER or doctor/physician.
P370 + P376	In case of fire: Stop leak if safe to Do so.
P370 + P378	In case of fire:
P370 + P380	In case of fire: Evacuate area.
P370 + P380 + P375	In case of fire: Evacuate area. Fight fire remotely due to the risk of explosion.
P371 + P380 + P375	In case of major fire and large quantities: Evacuate area. Fight fire remotely due to the risk of explosion.
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P402 + P404	Store in a dry place. Store in a closed container.
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Physical hazards
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CAS No.: 59969-65-2

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CAS No.: 59969-65-2

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Product Details of [ 59969-65-2 ]

Safety of [ 59969-65-2 ]

Application In Synthesis of [ 59969-65-2 ]

[ 59969-65-2 ] Synthesis Path-Downstream 1~35

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Technical Information

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