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Chemical Structure| 5765-65-1 Chemical Structure| 5765-65-1

Structure of 5765-65-1

Chemical Structure| 5765-65-1

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Product Details of [ 5765-65-1 ]

CAS No. :5765-65-1
Formula : C11H13NO3
M.W : 207.23
SMILES Code : O=C(ON1CCOCC1)C2=CC=CC=C2
MDL No. :MFCD09032166
InChI Key :ZTURCWOWVLVNPE-UHFFFAOYSA-N
Pubchem ID :11252758

Safety of [ 5765-65-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 5765-65-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 5765-65-1 ]

[ 5765-65-1 ] Synthesis Path-Downstream   1~12

  • 1
  • [ 5765-65-1 ]
  • n-octyl-Mg-X [ No CAS ]
  • [ 13063-60-0 ]
  • 2
  • [ 5765-65-1 ]
  • [ 5572-94-1 ]
  • [ 87350-77-4 ]
  • 4
  • [ 5765-65-1 ]
  • [ 73183-34-3 ]
  • [ 25015-63-8 ]
  • [ 175278-00-9 ]
  • (o-trifluoromethoxy-o'-morpholino)phenyl pinacol boronate ester [ No CAS ]
  • C11H12F3NO2 [ No CAS ]
  • 5
  • [ 5765-65-1 ]
  • [ 73183-34-3 ]
  • [ 175278-00-9 ]
  • (o-trifluoromethoxy-o'-morpholino)phenyl pinacol boronate ester [ No CAS ]
  • 6
  • [ 5765-65-1 ]
  • [ 615-37-2 ]
  • [ 1719-19-3 ]
  • 4-(3-methyl-2-(phenylethynyl)phenyl)morpholine [ No CAS ]
YieldReaction ConditionsOperation in experiment
96% With norbornene; palladium diacetate; caesium carbonate; triphenylphosphine; In 1,4-dioxane; at 100℃; for 18h;Inert atmosphere; Schlenk technique; In a dry 25 mL Schlenk reaction tube, add 109 mg of o-methyliodobenzene, 114 mg of benzoyloxymorpholine, 96 mg of 2-methyl-4-phenyl-3-butyn-2-ol,11mg of palladium acetate, 26mg of triphenylphosphine, 94mg of norbornene,489mg of cesium carbonate and 2.5mL of 1,4-dioxane. Under the protection of nitrogen,Stir at 100 C for 18 hours. After the reaction, cool to room temperature,Directly through the silica gel column (the body of ethyl acetate and petroleum ether(Product ratio is 1:30), to obtain 133mg of product, yield 96%,
  • 7
  • [ 5765-65-1 ]
  • [ 120315-65-3 ]
  • C12H14N2O2 [ No CAS ]
  • 8
  • [ 5765-65-1 ]
  • [ 43192-34-3 ]
  • C12H15NO3 [ No CAS ]
  • 9
  • [ 5765-65-1 ]
  • [ 924869-17-0 ]
  • [ 88284-48-4 ]
  • methyl 2-(2-morpholinophenyl)benzo[d]oxazole-5-carboxylate [ No CAS ]
  • 10
  • [ 5765-65-1 ]
  • [ 14547-73-0 ]
  • N-(4-bromo-2-morpholinophenyl)picolinamide [ No CAS ]
  • 11
  • [ 5765-65-1 ]
  • [ 775-56-4 ]
  • [ 92-53-5 ]
  • 12
  • [ 5765-65-1 ]
  • [ 591-87-7 ]
  • [ 103962-05-6 ]
  • (E)-3-(2,6-dimorpholino-4-(trifluoromethoxy)phenyl)allyl acetate [ No CAS ]
YieldReaction ConditionsOperation in experiment
40% With norborn-2-ene; trifuran-2-yl-phosphane; caesium carbonate; palladium dichloride; In toluene; at 80℃; for 24h;Inert atmosphere; Palladium chloride 0.01mmol, tris(2-furyl)phosphine 0.025mmol, norbornene 0.2mmol, cesium carbonate 0.25mmol, <strong>[103962-05-6]1-iodo-4-(trifluoromethoxy)benzene</strong> 0.1mmol, morpholin-4-yl benzoate Add 0.2 mmol of allyl acetate, and 1 mL of toluene into a 15 mL reaction tube, fill it with nitrogen repeatedly 10 times, place it in an oil bath at 80C, and react for 24 hours; cool to room temperature, filter, concentrate, and thin-layer chromatography 17.3mg of the target product was obtained through purification, with a yield of 40%.
 

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[ 5765-65-1 ]

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