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Chemical Structure| 55899-45-1 Chemical Structure| 55899-45-1

Structure of 55899-45-1

Chemical Structure| 55899-45-1

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Product Details of [ 55899-45-1 ]

CAS No. :55899-45-1
Formula : C9H10N2
M.W : 146.19
SMILES Code : NC1=CC=CC2=C1NC(C)=C2

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Application In Synthesis of [ 55899-45-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 55899-45-1 ]

[ 55899-45-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 41018-86-4 ]
  • [ 55899-45-1 ]
  • [ 101832-73-9 ]
YieldReaction ConditionsOperation in experiment
70% a) 2,3-Dimethyl-7-aminoindole (Compound 35A13-A) The title compound was prepared as described for Compound 35A1-A starting from 2,3-dimethyl-7-nitroindole (N. Moskalev et al, Tetrahedron Letters 40, 5395-5398, (1999)) instead of 2-methyl-7-nitroindole. The crude was purified by flash chromatography eluding with petroleum ether-ethyl acetate 7:3 to give the title compound (70%). 1H-NMR (δ): 2.31 (s, 3H), 2.49 (s, 3H), 3,85-4.21 (br, 2H), 6.27 (dd, 11H), 6.70 (dd, 1H), 6.94 (dd, 1H), 7.48-7.73 (br 1H)
 

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