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Chemical Structure| 52898-32-5 Chemical Structure| 52898-32-5

Structure of 52898-32-5

Chemical Structure| 52898-32-5

N-(3-Buten-1-yl)phthalimide

CAS No.: 52898-32-5

4.5 *For Research Use Only !

Cat. No.: A139786 Purity: 98%

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Product Details of [ 52898-32-5 ]

CAS No. :52898-32-5
Formula : C12H11NO2
M.W : 201.22
SMILES Code : O=C1N(CCC=C)C(C2=C1C=CC=C2)=O
MDL No. :MFCD00175471
InChI Key :ZDOLXCKKXHSEJG-UHFFFAOYSA-N
Pubchem ID :339432

Safety of [ 52898-32-5 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H319
Precautionary Statements:P305+P351+P338

Application In Synthesis of [ 52898-32-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 52898-32-5 ]

[ 52898-32-5 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 52898-32-5 ]
  • [ 16870-28-3 ]
  • 4-[(E)-4-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-but-1-enyl]-2-hydroxy-benzoic acid [ No CAS ]
  • 2
  • [ 959121-99-4 ]
  • [ 52898-32-5 ]
  • C22H18N2O3 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With sodium acetate; palladium diacetate; triphenylphosphine; In N,N-dimethyl-formamide; at 120℃;Inert atmosphere; General procedure: To a solution of 6-substituted or 7-substituted 3-bromoquinoline (17-23, 1.0 mmol), N-(but-3-enyl)phthalimide (0.22 g, 1.1 mmol), NaOAc (0.14 g, 2.0 mmol) and PPh3 (31 mg, 0.12 mmol) in 4 mL of DMF was added Pd(OAc)2 (9 mg, 0.04 mmol) at room temperature under Ar condition. The mixture was heated to 120 C and stirred at 120 C overnight. The reaction solution was allowed to cool to room temperature and diluted with 100 mL of DCM, washed with brine (6×100 mL), dried with Na2SO4, concentrated in vacuo. The residue was purified by column chromatography on silica gel (PE: EA = 4: 1) to give 24-30, as a white solid.
 

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[ 52898-32-5 ]

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