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Chemical Structure| 4383-22-6 Chemical Structure| 4383-22-6

Structure of 4383-22-6

Chemical Structure| 4383-22-6

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Product Details of [ 4383-22-6 ]

CAS No. :4383-22-6
Formula : C10H13N
M.W : 147.22
SMILES Code : C=CCNCC1=CC=CC=C1
MDL No. :MFCD00463446
InChI Key :RHUCQDQRNUUMKY-UHFFFAOYSA-N
Pubchem ID :521150

Safety of [ 4383-22-6 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H314
Precautionary Statements:P280-P305+P351+P338-P310
Class:8
UN#:3267
Packing Group:

Application In Synthesis of [ 4383-22-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 4383-22-6 ]

[ 4383-22-6 ] Synthesis Path-Downstream   1~7

  • 3
  • [ 4383-22-6 ]
  • [ 111771-08-5 ]
  • [ 1050203-43-4 ]
YieldReaction ConditionsOperation in experiment
67% A mixture of <strong>[111771-08-5]2-fluoro-6-iodobenzoic acid</strong> (Intermediate A, 30 g, 112.78 mmol) in SOCl2 (60 mL) was heated at 800C for 1.5 h. Excess SOCl2 was removed in vacuo and the residue obtained was added to a solution of triethylamine (13.7 g, 135.64 mmol) in THF (50 mL). This solution was added dropwise to a solution of N-benzylprop-2-en- 1-amine (Intermediate B,16.6 g, 112.93 mmol) in THF (15OmL) cooled to 5C. The resulting solution stirred at RT for 2 h. The mixture was concentrated and the residue was dissolved in EtOAc (200 mL). The organic layer was washed with aqueous NaHSO4 (2x50 mL), aqueous NaHCO3 (1x50 mL), and brine (1x50 mL), dried over Na2SO4, and evaporated to dryness to afford 30.0 g (67%) of N-allyl-N-benzyl-2- fluoro-6-iodobenzamide as a white solid.
  • 4
  • [ 4383-22-6 ]
  • [ 51307-59-6 ]
  • [ 1401332-25-9 ]
  • 5
  • [ 4383-22-6 ]
  • [ 51307-59-6 ]
  • [ 1453196-49-0 ]
  • 6
  • [ 4383-22-6 ]
  • [ 30982-08-2 ]
  • [ 503155-50-8 ]
  • 7
  • [ 4383-22-6 ]
  • [ 31161-46-3 ]
  • 2,2,2-trifluoro-1-((methoxycarbonyl)amino)ethyl acetate [ No CAS ]
  • methyl 5-((5-benzoylthiophen-2-yl)methyl)-3-benzyl-2-(trifluoromethyl)imidazolidine-1-carboxylate [ No CAS ]
 

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Related Functional Groups of
[ 4383-22-6 ]

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