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Chemical Structure| 41276-30-6 Chemical Structure| 41276-30-6

Structure of 41276-30-6

Chemical Structure| 41276-30-6

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Product Details of [ 41276-30-6 ]

CAS No. :41276-30-6
Formula : C15H19NO3
M.W : 261.32
SMILES Code : CCOC(=O)C1CN(CC2=CC=CC=C2)CCC1=O
MDL No. :MFCD00792540
InChI Key :ROSZJQBQGFBFSW-UHFFFAOYSA-N
Pubchem ID :102624

Safety of [ 41276-30-6 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H332-H335
Precautionary Statements:P233-P260-P261-P264-P270-P271-P280-P301+P312-P302+P352-P304-P304+P340-P305+P351+P338-P312-P321-P330-P332+P313-P337+P313-P340-P362-P403-P403+P233-P405-P501

Application In Synthesis of [ 41276-30-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 41276-30-6 ]

[ 41276-30-6 ] Synthesis Path-Downstream   1~4

  • 2
  • [ 41276-30-6 ]
  • [ 463-52-5 ]
  • [ 109229-22-3 ]
  • 3
  • [ 41276-30-6 ]
  • [ 3473-63-0 ]
  • [ 109229-22-3 ]
YieldReaction ConditionsOperation in experiment
55% With ethanol; sodium ethanolate;Reflux; Preparation 16-Benz i-5,6,7,8-tetrah dropyrido[4,3-rf]pyrimidin-4 3H)-Sodium methylate (43 g, 0.8 mol) was added to a mixture of imidoformamide acetate (39.85 g, 0.383 mol) and ethyl l-benzyl-4-oxopiperidine-3-carboxylate (110 g, 0.37 mol) in absolute ethanol (250 mL). The reaction mixture was refluxed for 3-4 h, during which time the course of the reaction was monitored by TLC (Merck UV-254; chloroform/methanol 4:1 ). The mixture was then filtered, and the filtrate was evaporated. Water (-400 mL) was added to the residue, and the obtained aqueous solution was acidified to pH 7-8. The product was then extracted with chloroform, and the extract was dried over MgS04 and evaporated to give the title compound in 55% (50.7 g) yield. The product was then recrystallized from ethylacetate.
  • 4
  • [ 41276-30-6 ]
  • [ 1056934-87-2 ]
 

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