Home Cart Sign in  
Chemical Structure| 29655-79-6 Chemical Structure| 29655-79-6

Structure of 29655-79-6

Chemical Structure| 29655-79-6

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 29655-79-6 ]

CAS No. :29655-79-6
Formula : C8H13NO5
M.W : 203.19
SMILES Code : C(C)OC(C(=O)NCC(=O)OCC)=O
MDL No. :MFCD00831071
InChI Key :WFXMDHFQXBWTSB-UHFFFAOYSA-N
Pubchem ID :2779372

Safety of [ 29655-79-6 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302-H319-H372-H410
Precautionary Statements:P260-P264-P273-P301+P312-P305+P351+P338-P314
Class:9
UN#:3082
Packing Group:

Application In Synthesis of [ 29655-79-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 29655-79-6 ]

[ 29655-79-6 ] Synthesis Path-Upstream   1~7

  • 1
  • [ 623-33-6 ]
  • [ 4755-77-5 ]
  • [ 29655-79-6 ]
YieldReaction ConditionsOperation in experiment
51% With triethylamine In dichloromethane Example 2 Ii; Compound 4 was prepared according to the Ref: J. Hetero. Chem. 1995, 32, 1693-1702. Then, it was reduced by NaBH4ZLiCl in ethanol solution. Further oxidation by Dess-Martin reagent gave the desired aldehyde 6 in 25 percent overall two-step yield.
References: [1] Synthetic Communications, 2000, vol. 30, # 17, p. 3171 - 3180.
[2] Patent: WO2007/124546, 2007, A1, . Location in patent: Page/Page column 63.
[3] Chemische Berichte, 1897, vol. 30, p. 590.
[4] Journal of the American Chemical Society, 1997, vol. 119, # 1, p. 86 - 93.
[5] Organic Process Research and Development, 2004, vol. 8, # 2, p. 192 - 200.
  • 2
  • [ 95-92-1 ]
  • [ 459-73-4 ]
  • [ 29655-79-6 ]
References: [1] Bioorganic and Medicinal Chemistry Letters, 2002, vol. 12, # 8, p. 1203 - 1208.
[2] Acta Chemica Scandinavica, 1999, vol. 53, # 7, p. 521 - 527.
  • 3
  • [ 924-44-7 ]
  • [ 29655-79-6 ]
YieldReaction ConditionsOperation in experiment
60% With ammonium acetate In tetrahydrofuran at 66℃; for 8 h; General procedure: To the solution of isopropyl glyoxylate (1.28 g, 11 mmol) in THF (50 mL), ammonium acetate (3 equiv., 2.55 g, 33 mmol) was added and refluxed for 8 h. The solvent was evaporated under vacuum and product was obtained on purification through column chromatography on silica gel.
References: [1] Tetrahedron Letters, 2017, vol. 58, # 19, p. 1891 - 1894.
  • 4
  • [ 623-33-6 ]
  • [ 95-92-1 ]
  • [ 29655-79-6 ]
References: [1] Journal of Heterocyclic Chemistry, 1995, vol. 32, # 6, p. 1693 - 1702.
  • 5
  • [ 4755-77-5 ]
  • [ 29655-79-6 ]
References: [1] Patent: US2002/35115, 2002, A1, .
  • 6
  • [ 64-17-5 ]
  • [ 144-62-7 ]
  • [ 56-40-6 ]
  • [ 29655-79-6 ]
References: [1] Bulletin of the Chemical Society of Japan, 1972, vol. 45, p. 1917 - 1918.
  • 7
  • [ 29655-79-6 ]
  • [ 221136-66-9 ]
References: [1] Bioorganic and Medicinal Chemistry Letters, 2002, vol. 12, # 8, p. 1203 - 1208.
[2] Synthetic Communications, 2000, vol. 30, # 17, p. 3171 - 3180.
 

Historical Records