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Chemical Structure| 28746-99-8 Chemical Structure| 28746-99-8

Structure of 28746-99-8

Chemical Structure| 28746-99-8

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Product Details of [ 28746-99-8 ]

CAS No. :28746-99-8
Formula : C12H20O2
M.W : 196.29
SMILES Code : O=C1C(C2(O)CCCCC2)CCCC1
MDL No. :MFCD03837683
InChI Key :AERVJOBGBMEFDV-UHFFFAOYSA-N
Pubchem ID :566680

Safety of [ 28746-99-8 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 28746-99-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 28746-99-8 ]

[ 28746-99-8 ] Synthesis Path-Downstream   1~27

  • 7
  • [ 28746-99-8 ]
  • [ 1502-22-3 ]
  • [ 108-94-1 ]
  • 8
  • [ 2612-42-2 ]
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  • [ 38329-94-1 ]
  • 9
  • [ 1068-55-9 ]
  • [ 108-94-1 ]
  • [ 3552-01-0 ]
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  • 10
  • [ 108-94-1 ]
  • [ 74636-49-0 ]
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  • 11
  • [ 108-94-1 ]
  • [ 2888-11-1 ]
  • [ 24344-21-6 ]
  • [ 28746-99-8 ]
  • 13
  • [ 71444-26-3 ]
  • [ 108-94-1 ]
  • [ 28746-99-8 ]
  • 14
  • [ 108-94-1 ]
  • [ 17851-97-7 ]
  • [ 28746-99-8 ]
  • 15
  • [ 17851-97-7 ]
  • [ 100-44-7 ]
  • [ 946-33-8 ]
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  • 16
  • [ 6651-36-1 ]
  • [ 108-94-1 ]
  • [ 28746-99-8 ]
  • 18
  • [ 140112-10-3 ]
  • [ 120-92-3 ]
  • [ 28746-99-8 ]
  • 2-(1-hydroxycyclopentyl)-cyclohexanone [ No CAS ]
  • 19
  • [ 140112-10-3 ]
  • [ 67-64-1 ]
  • [ 28746-99-8 ]
  • [ 3304-23-2 ]
  • 20
  • [ 140112-10-3 ]
  • [ 502-42-1 ]
  • 2-(1-hydroxy-cycloheptyl)-cyclohexanone [ No CAS ]
  • [ 28746-99-8 ]
  • 21
  • [ 108-94-1 ]
  • 1-halo-2-bromo-4-fluorobenzene [ No CAS ]
  • [ 28746-99-8 ]
  • 22
  • [ 56974-20-0 ]
  • [ 28746-99-8 ]
  • 23
  • [ 10468-40-3 ]
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  • 24
  • [ 108-94-1 ]
  • [ 1502-22-3 ]
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  • 25
  • [ 54673-30-2 ]
  • [ 28746-99-8 ]
  • [ 1266333-69-0 ]
  • 26
  • [ 108-94-1 ]
  • [ 1502-22-3 ]
  • [ 1011-12-7 ]
  • [ 28746-99-8 ]
  • [ 52897-78-6 ]
  • C18H28O2 [ No CAS ]
  • C18H26O [ No CAS ]
YieldReaction ConditionsOperation in experiment
With sodium hydroxide; at 20℃; for 72h; Dodecahydrotriphenylene (2). Calcined anhydrous sodiumhydroxide (6 g, 0.15 mol) was added to anhydrous freshly distilled cyclohexanone (60 mL, 0.58 mol) and the mixture obtained was stirred at room temperature for three days. Then, water (150 mL) was added to the reaction mixture with stirring, a precipitate was filtered off, washed with 10% aqueous HCl and water, and dried. The mixture of intermediate products without additional purification was added to polyphosphoric acid (40 g) and stirred for 2 h at 150 C. Then, the reaction mixture was mixed with anhydrous sodium sulfate (100 g), placed into a Soxhlet extractor, and the product was continuously extracted with light petroleum (b.p. 40-70 C). A precipitate was filtered off, washed with hexane, and dried. The yield was 24 g (52%),
  • 27
  • [ 75-77-4 ]
  • [ 6651-36-1 ]
  • [ 124-38-9 ]
  • [ 74-88-4 ]
  • [ 28746-99-8 ]
  • [ 10416-74-7 ]
  • [ 108-94-1 ]
  • [ 583-60-8 ]
 

Historical Records

Technical Information

• Appel Reaction • Baeyer-Villiger Oxidation • Barbier Coupling Reaction • Baylis-Hillman Reaction • Bucherer-Bergs Reaction • Buchwald-Hartwig C-N Bond and C-O Bond Formation Reactions • Chugaev Reaction • Clemmensen Reduction • Corey-Bakshi-Shibata (CBS) Reduction • Corey-Chaykovsky Reaction • Corey-Kim Oxidation • Dess-Martin Oxidation • Fischer Indole Synthesis • Grignard Reaction • Halogenation • Heat of Combustion • Henry Nitroaldol Reaction • Horner-Wadsworth-Emmons Reaction • Hydride Reductions • Jones Oxidation • Lawesson's Reagent • Leuckart-Wallach Reaction • Martin's Sulfurane Dehydrating Reagent • McMurry Coupling • Meerwein-Ponndorf-Verley Reduction • Mitsunobu Reaction • Moffatt Oxidation • Oxidation of Alcohols by DMSO • Passerini Reaction • Paternò-Büchi Reaction • Petasis Reaction • Peterson Olefination • Pictet-Spengler Tetrahydroisoquinoline Synthesis • Preparation of Alcohols • Preparation of Aldehydes and Ketones • Preparation of Amines • Prins Reaction • Reactions of Alcohols • Reactions of Aldehydes and Ketones • Reactions of Amines • Reactions with Organometallic Reagents • Reformatsky Reaction • Ritter Reaction • Robinson Annulation • Schlosser Modification of the Wittig Reaction • Schmidt Reaction • Sharpless Olefin Synthesis • Specialized Acylation Reagents-Ketenes • Stobbe Condensation • Swern Oxidation • Tebbe Olefination • Ugi Reaction • Wittig Reaction • Wolff-Kishner Reduction

Categories

Related Functional Groups of
[ 28746-99-8 ]

Aliphatic Cyclic Hydrocarbons

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