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Chemical Structure| 1502-22-3 Chemical Structure| 1502-22-3
Chemical Structure| 1502-22-3

[1,1'-Bi(cyclohexan)]-1'-en-2-one

CAS No.: 1502-22-3

4.5 *For Research Use Only !

Cat. No.: A145509 Purity: 85%

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Product Details of [ 1502-22-3 ]

CAS No. :1502-22-3
Formula : C12H18O
M.W : 178.27
SMILES Code : O=C1C(C2=CCCCC2)CCCC1
MDL No. :MFCD00013796
InChI Key :GVNVAWHJIKLAGL-UHFFFAOYSA-N
Pubchem ID :101175

Safety of [ 1502-22-3 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P233-P260-P261-P264-P271-P280-P302+P352-P304-P304+P340-P305+P351+P338-P312-P321-P332+P313-P337+P313-P340-P362-P403-P403+P233-P405-P501

Application In Synthesis of [ 1502-22-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1502-22-3 ]

[ 1502-22-3 ] Synthesis Path-Downstream   1~6

  • 4
  • [ 28746-99-8 ]
  • [ 1502-22-3 ]
  • [ 108-94-1 ]
  • 5
  • [ 108-94-1 ]
  • [ 1502-22-3 ]
  • [ 28746-99-8 ]
  • 6
  • [ 108-94-1 ]
  • [ 1502-22-3 ]
  • [ 1011-12-7 ]
  • [ 28746-99-8 ]
  • [ 52897-78-6 ]
  • C18H28O2 [ No CAS ]
  • C18H26O [ No CAS ]
YieldReaction ConditionsOperation in experiment
With sodium hydroxide; at 20℃; for 72h; Dodecahydrotriphenylene (2). Calcined anhydrous sodiumhydroxide (6 g, 0.15 mol) was added to anhydrous freshly distilled cyclohexanone (60 mL, 0.58 mol) and the mixture obtained was stirred at room temperature for three days. Then, water (150 mL) was added to the reaction mixture with stirring, a precipitate was filtered off, washed with 10% aqueous HCl and water, and dried. The mixture of intermediate products without additional purification was added to polyphosphoric acid (40 g) and stirred for 2 h at 150 C. Then, the reaction mixture was mixed with anhydrous sodium sulfate (100 g), placed into a Soxhlet extractor, and the product was continuously extracted with light petroleum (b.p. 40-70 C). A precipitate was filtered off, washed with hexane, and dried. The yield was 24 g (52%),
 

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