27982-06-5|(4-Ethoxyphenyl)(phenyl)methanone| Ambeed

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Quality Control of [ 27982-06-5 ] Purity: 95% SDS Specification

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Product Details of [ 27982-06-5 ]

CAS No. :	27982-06-5
Formula :	C₁₅H₁₄O₂
M.W :	226.27
SMILES Code :	O=C(C1=CC=C(OCC)C=C1)C2=CC=CC=C2
MDL No. :	MFCD00568422
InChI Key :	IBRIFDGHXDFGBY-UHFFFAOYSA-N
Pubchem ID :	248129

Safety of [ 27982-06-5 ]

GHS Pictogram:
Signal Word:	Warning
Hazard Statements:	H302-H315-H319
Precautionary Statements:	P261-P305+P351+P338

Application In Synthesis of [ 27982-06-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 27982-06-5 ]

[ 27982-06-5 ] Synthesis Path-Downstream 1~35

1
[ 109-06-8 ]
[ 27982-06-5 ]
1-(4-ethoxy-phenyl)-1-phenyl-2-[2]pyridyl-ethanol [ No CAS ]

References: [1]Journal of the American Chemical Society,1954,vol. 76,p. 2431,2435, 2438.
Journal of the American Chemical Society,1957,vol. 79,p. 6575.

2
[ 10467-10-4 ]
[ 27982-06-5 ]
4-(1-phenyl-propenyl)-phenetole [ No CAS ]

References: [1]Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences,1910,vol. 151,p. 517.

3
[ 917-64-6 ]
[ 27982-06-5 ]
[ 17772-45-1 ]

References: [1]Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences,1910,vol. 151,p. 517.
[2]Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences,1910,vol. 151,p. 517.

4
[ 27982-06-5 ]
[ 151-50-8 ]
[ 1066-33-7 ]
[ 86029-57-4 ]

References: [1]Patent: US2687416,1951,A .

5
[ 27982-06-5 ]
phenylmagnesium bromide [ No CAS ]
[ 62345-22-6 ]

References: [1]Journal of the Chemical Society,1957,p. 4240,4241.

6
[ 27982-06-5 ]
[ 34979-36-7 ]

References: [1]Recueil des Travaux Chimiques des Pays-Bas,1920,vol. 39,p. 345.
Recueil des Travaux Chimiques des Pays-Bas,1922,vol. 41,p. 717.
[2]Recueil des Travaux Chimiques des Pays-Bas,1920,vol. 39,p. 345.
Recueil des Travaux Chimiques des Pays-Bas,1922,vol. 41,p. 717.
[3]Asian Journal of Chemistry,2018,vol. 30,p. 821 - 826.
[4]Pharmaceuticals,2021,vol. 14,p. 1 - 59.

7
[ 27982-06-5 ]
[ 35672-52-7 ]

References: [1]Chemische Berichte,1898,vol. 31,p. 1003.

8
[ 27982-06-5 ]
1,2-bis-(4-ethoxy-phenyl)-1,2-diphenyl-ethane-1,2-diol [ No CAS ]

References: [1]Journal of the American Chemical Society,1934,vol. 56,p. 2081,2083.
[2]Journal of the American Chemical Society,1934,vol. 56,p. 2081,2083.
[3]Journal of the American Chemical Society,1934,vol. 56,p. 2081,2083.

9
[ 27982-06-5 ]
[ 871893-40-2 ]

References: [1]Recueil des Travaux Chimiques des Pays-Bas,1922,vol. 41,p. 718.
Recueil des Travaux Chimiques des Pays-Bas,1923,vol. 42,p. 506.

10
[ 27982-06-5 ]
[ 860564-39-2 ]

References: [1]Recueil des Travaux Chimiques des Pays-Bas,1930,vol. 49,p. 383,387.

11
[ 27982-06-5 ]
4'-ethoxy-2,3',5'-trinitro-benzophenone [ No CAS ]

References: [1]Recueil des Travaux Chimiques des Pays-Bas,1930,vol. 49,p. 383,387.

12
[ 27982-06-5 ]
[ 1137-42-4 ]

References: [1]Journal fur praktische Chemie (Leipzig 1954),1937,vol. <2> 147,p. 293,303.

13
[ 951884-62-1 ]
[ 27982-06-5 ]

References: [1]Recueil des Travaux Chimiques des Pays-Bas,1920,vol. 39,p. 345.
Recueil des Travaux Chimiques des Pays-Bas,1922,vol. 41,p. 717.

14
[ 98-88-4 ]
[ 103-73-1 ]
[ 27982-06-5 ]

Yield	Reaction Conditions	Operation in experiment
92%	With bismuth(lll) trifluoromethanesulfonate; In neat (no solvent); at 100℃; for 0.166667h;Sealed tube; Microwave irradiation;	General procedure: A 10-mL pressurized glass tube with Teflon-coated septum equipped with amagnetic stirrer was charged with substrate (1 mmol), benzoyl chloride (1 mmol),and metal triflate (0.1 equiv). The tube was sealed and placed into a CEM microwaveat the temperature for the appropriate time. The reaction mixture was allowed tocool to the room temperature in the MW oven. After cooling, water (15 mL) wasadded to the mixture and the product was extracted by ethyl acetate or dichloromethane,which gave similar results (315mL). The organic layer was decanted;washed with water, aqueous NaHCO3, and brine; and dried with MgSO4. Thesolvent was then removed on a rotary evaporator and subjected to flash chromatographyon silica gel (mixture of hexane and ethyl acetate solvent to elute theproduct). The fractions containing product were concentrated and dried undervacuum to yield pure product. All products are known compounds; the purity and identityof all products were confirmed by GC-MS and 1H and 13C NMR spectroscopy.

References: [1]Dalton Transactions,2016,vol. 45,p. 7875 - 7880.
[2]Synthetic Communications,2014,vol. 44,p. 2921 - 2929.
[3]Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry,2011,vol. 50,p. 1192 - 1195.
[4]Advanced Synthesis and Catalysis,2004,vol. 346,p. 599 - 602.
[5]Revue Roumaine de Chimie,2003,vol. 48,p. 175 - 177.
[6]Chemische Berichte,1890,vol. 23,p. 1202.
[7]Patent: US2475567,1946,A .
[8]Chemische Berichte,1890,vol. 23,p. 1202.
[9]Patent: US2468762,1946,A .

15
[ 98-88-4 ]
[ 103-73-1 ]
[ 27982-06-5 ]
[ 127154-52-3 ]

References: [1]Journal of the Chemical Society,1936,p. 1854,1855.

16
[ 27982-06-5 ]
[ 6921-34-2 ]
[ 856066-40-5 ]

References: [1]Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences,1910,vol. 151,p. 517.

17
[ 27982-06-5 ]
[ 100555-98-4 ]

References: [1]Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry,1985,vol. 24,p. 312.

18
[ 1144-74-7 ]
[ 141-52-6 ]
[ 27982-06-5 ]

References: [1]Tetrahedron,1993,vol. 49,p. 4463 - 4476.

19
[ 27982-06-5 ]
[ 1576-35-8 ]
[ 100556-03-4 ]

References: [1]Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry,1985,vol. 24,p. 312.

20
[ 611-94-9 ]
[ 64-17-5 ]
[ 27982-06-5 ]

References: [1]Journal of Organic Chemistry,1998,vol. 63,p. 4510 - 4514.

Yield	Reaction Conditions	Operation in experiment
		The following benzophenones and benzhydrols are representative of compounds which are useful in the practice of the present invention: ... 3-bromo-4'-chlorobenzophenone 2-n-propyl-3'-chlorobenzophenone 3,3'-dichloro-2-nitrobenzophenone 3-chloro-3'-methylbenzophenone 4-ethoxybenzophenone 3-diethylcarbamoylbenzophenone 2-hydroxy-3',5'-dichlorobenzophenone 3-trifluoromethylbenzophenone ...

23
[ 27982-06-5 ]
alcoholic KOH-solution [ No CAS ]
[ 34979-36-7 ]

References: [1]Recueil des Travaux Chimiques des Pays-Bas,1920,vol. 39,p. 345.
Recueil des Travaux Chimiques des Pays-Bas,1922,vol. 41,p. 717.

24
[ 64-17-5 ]
[ 27982-06-5 ]
sodium [ No CAS ]
[ 35672-52-7 ]

References: [1]Chemische Berichte,1898,vol. 31,p. 1003.

25
[ 951884-62-1 ]
alcoholic KOH-solution [ No CAS ]
[ 27982-06-5 ]

References: [1]Recueil des Travaux Chimiques des Pays-Bas,1920,vol. 39,p. 345.
Recueil des Travaux Chimiques des Pays-Bas,1922,vol. 41,p. 717.

26
4-(1,2-dimethyl-1-phenyl-allyl)-phenetole [ No CAS ]
[ 64-19-7 ]
CrO₃ [ No CAS ]
[ 27982-06-5 ]
[ 619-86-3 ]

References: [1]Annales de Chimie (Cachan, France),1913,vol. <8> 30,p. 396.

27
[ 27982-06-5 ]
4-ethoxy-3-bromo-benzhydrol [ No CAS ]

References: [1]Recueil des Travaux Chimiques des Pays-Bas,1922,vol. 41,p. 718.
Recueil des Travaux Chimiques des Pays-Bas,1923,vol. 42,p. 506.

28
[ 27982-06-5 ]
4'-methylamino-2,3',5'-trinitro-benzophenone [ No CAS ]

References: [1]Recueil des Travaux Chimiques des Pays-Bas,1930,vol. 49,p. 383,387.

29
[ 27982-06-5 ]
4-methylamino-3,5,3'-trinitro-benzophenone [ No CAS ]

References: [1]Recueil des Travaux Chimiques des Pays-Bas,1930,vol. 49,p. 383,387.

30
[ 27982-06-5 ]
4-(2-bromo-1-phenyl-propenyl)-phenetole [ No CAS ]

References: [1]Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences,1910,vol. 151,p. 517.

31
[ 27982-06-5 ]
[ 860756-32-7 ]

References: [1]Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences,1910,vol. 151,p. 517.

32
[ 103-73-1 ]
[ 27982-06-5 ]

References: [1]Recueil des Travaux Chimiques des Pays-Bas,1920,vol. 39,p. 345.
Recueil des Travaux Chimiques des Pays-Bas,1922,vol. 41,p. 717.

33
[ 1711-02-0 ]
[ 27982-06-5 ]

References: [1]Recueil des Travaux Chimiques des Pays-Bas,1920,vol. 39,p. 345.
Recueil des Travaux Chimiques des Pays-Bas,1922,vol. 41,p. 717.

34
[ 64-17-5 ]
[ 345-83-5 ]
[ 27982-06-5 ]

References: [1]Journal of Organic Chemistry,2020,vol. 85,p. 11181 - 11189.
[2]Synthetic Communications,2010,vol. 40,p. 2122 - 2129.

35
[ 591-50-4 ]
[ 201230-82-2 ]
[ 22237-13-4 ]
[ 27982-06-5 ]

Yield	Reaction Conditions	Operation in experiment
	With potassium carbonate; at 100℃; under 7500.75 Torr; for 8h;Autoclave;	Carbonylative Suzuki coupling reactions All of the carbonylative Suzuki coupling reactions were conducted in a sealed stainless steel reaction kettle. Arylboronic acid (1.5 mmol), aryl iodide (1.0 mmol), base (3.0 mmol), 3 wt% Pd/SiC and anisole (10 mL) were added to the reaction kettle, and the resulting mixture was placed under a certain pressure of CO. All of the reactions were conducted over several hours at certain temperatures. The products of the reactions were analyzed by GC-MS on a Bruker SCION SQ 456 GC-MS system (Karlsruhe, Germany).

References: [1]Chinese Journal of Catalysis,2015,vol. 36,p. 322 - 327.

Historical Records

Technical Information

• Baeyer-Villiger Oxidation • Barbier Coupling Reaction • Baylis-Hillman Reaction • Benzylic Oxidation • Birch Reduction • Blanc Chloromethylation • Bucherer-Bergs Reaction • Clemmensen Reduction • Corey-Bakshi-Shibata (CBS) Reduction • Corey-Chaykovsky Reaction • Fischer Indole Synthesis • Friedel-Crafts Reaction • Grignard Reaction • Henry Nitroaldol Reaction • Horner-Wadsworth-Emmons Reaction • Hydride Reductions • Hydrogenolysis of Benzyl Ether • Lawesson's Reagent • Leuckart-Wallach Reaction • McMurry Coupling • Meerwein-Ponndorf-Verley Reduction • Nomenclature of Ethers • Passerini Reaction • Paternò-Büchi Reaction • Petasis Reaction • Peterson Olefination • Pictet-Spengler Tetrahydroisoquinoline Synthesis • Preparation of Aldehydes and Ketones • Preparation of Alkylbenzene • Preparation of Amines • Preparation of Ethers • Prins Reaction • Reactions of Aldehydes and Ketones • Reactions of Amines • Reactions of Benzene and Substituted Benzenes • Reactions of Ethers • Reformatsky Reaction • Robinson Annulation • Schlosser Modification of the Wittig Reaction • Schmidt Reaction • Specialized Acylation Reagents-Ketenes • Stobbe Condensation • Tebbe Olefination • Ugi Reaction • Vilsmeier-Haack Reaction • Wittig Reaction • Wolff-Kishner Reduction

Related Functional Groups of
[ 27982-06-5 ]

Aryls

A176903 [52886-92-7]

(4-Ethoxyphenyl)(4-methoxyphenyl)methanone

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Ethers

A176903 [52886-92-7]

(4-Ethoxyphenyl)(4-methoxyphenyl)methanone

Similarity: 1.00

A114894 [14814-17-6]

(4-(2-Hydroxyethoxy)phenyl)(phenyl)methanone

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Ketones

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(4-Ethoxyphenyl)(4-methoxyphenyl)methanone

Similarity: 1.00

A114894 [14814-17-6]

(4-(2-Hydroxyethoxy)phenyl)(phenyl)methanone

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H371	May cause damage to organs
H372	Causes damage to organs through prolonged or repeated exposure
H373	May cause damage to organs through prolonged or repeated exposure
Environmental hazards
Code	Phrase
H400	Very toxic to aquatic life
H401	Toxic to aquatic life
H402	Harmful to aquatic life
H410	Very toxic to aquatic life with long-lasting effects
H411	Toxic to aquatic life with long-lasting effects
H412	Harmful to aquatic life with long-lasting effects
H413	May cause long-lasting harmful effects to aquatic life
H420	Harms public health and the environment by destroying ozone in the upper atmosphere

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CAS No.: 27982-06-5

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