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Chemical Structure| 103-73-1 Chemical Structure| 103-73-1

Structure of Phenetole
CAS No.: 103-73-1

Chemical Structure| 103-73-1

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Product Details of [ 103-73-1 ]

CAS No. :103-73-1
Formula : C8H10O
M.W : 122.16
SMILES Code : CCOC1=CC=CC=C1
MDL No. :MFCD00009090
InChI Key :DLRJIFUOBPOJNS-UHFFFAOYSA-N
Pubchem ID :7674

Safety of [ 103-73-1 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H225
Precautionary Statements:P210-P403+P235
Class:3
UN#:1993
Packing Group:

Application In Synthesis of [ 103-73-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 103-73-1 ]

[ 103-73-1 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 98-88-4 ]
  • [ 103-73-1 ]
  • [ 27982-06-5 ]
YieldReaction ConditionsOperation in experiment
92% With bismuth(lll) trifluoromethanesulfonate; In neat (no solvent); at 100℃; for 0.166667h;Sealed tube; Microwave irradiation; General procedure: A 10-mL pressurized glass tube with Teflon-coated septum equipped with amagnetic stirrer was charged with substrate (1 mmol), benzoyl chloride (1 mmol),and metal triflate (0.1 equiv). The tube was sealed and placed into a CEM microwaveat the temperature for the appropriate time. The reaction mixture was allowed tocool to the room temperature in the MW oven. After cooling, water (15 mL) wasadded to the mixture and the product was extracted by ethyl acetate or dichloromethane,which gave similar results (315mL). The organic layer was decanted;washed with water, aqueous NaHCO3, and brine; and dried with MgSO4. Thesolvent was then removed on a rotary evaporator and subjected to flash chromatographyon silica gel (mixture of hexane and ethyl acetate solvent to elute theproduct). The fractions containing product were concentrated and dried undervacuum to yield pure product. All products are known compounds; the purity and identityof all products were confirmed by GC-MS and 1H and 13C NMR spectroscopy.
  • 2
  • [ 98-88-4 ]
  • [ 103-73-1 ]
  • [ 27982-06-5 ]
  • [ 127154-52-3 ]
 

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