2239-31-8|(1-(Aminomethyl)cyclopentyl)methanol| Ambeed

Size	Price	VIP Price	US Stock	Global Stock	In Stock
{[ item.pr_size ]}		Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

{[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

Quality Control of [ 2239-31-8 ] Purity: 95% SDS Specification

COA

Search for reports by entering the product batch number.
Batch number can be found on the product's label following the word 'Batch'.

NMR

Search for reports by entering the product batch number.
Batch number can be found on the product's label following the word 'Batch'.

CNMR

Search for reports by entering the product batch number.
Batch number can be found on the product's label following the word 'Batch'.

HPLC

Search for reports by entering the product batch number.
Batch number can be found on the product's label following the word 'Batch'.

LC-MS

Search for reports by entering the product batch number.
Batch number can be found on the product's label following the word 'Batch'.

1-2 Day Shipping
High Quality
Technical Support

Product Details of [ 2239-31-8 ]

CAS No. :	2239-31-8
Formula :	C₇H₁₅NO
M.W :	129.20
SMILES Code :	NCC1(CO)CCCC1
MDL No. :	MFCD09864390
InChI Key :	WUROIEARWDBJIO-UHFFFAOYSA-N
Pubchem ID :	22379517

Safety of [ 2239-31-8 ]

GHS Pictogram:
Signal Word:	Warning
Hazard Statements:	H317-H319
Precautionary Statements:	P280-P305+P351+P338

Application In Synthesis of [ 2239-31-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 2239-31-8 ]

[ 2239-31-8 ] Synthesis Path-Downstream 1~21

1
[ 28247-14-5 ]
[ 2239-31-8 ]

References: [1]Bioorganic and Medicinal Chemistry Letters,1999,vol. 9,p. 369 - 374.
[2]Journal of medicinal chemistry,1972,vol. 15,p. 1003 - 1006.
[3]Advanced Synthesis and Catalysis,2014,vol. 356,p. 1113 - 1118.

2
[ 24424-99-5 ]
[ 2239-31-8 ]
[ 223763-91-5 ]

Yield	Reaction Conditions	Operation in experiment
15.9 g	With triethylamine; In tetrahydrofuran; at 20℃;	To a stirred solution of [1-(aminomethyl)cyclopentyl]methanol (50.7 g) in THF (304 mL) was added triethylamine(60.2 mL) under ice-cooling. Di-tert-butyl dicarbonate (94.2 g) in THF (101 mL) was added dropwise to this solution.After the addition, the reaction mixture was stirred at room temperature overnight. The reaction mixture was diluted withwater and ethyl acetate, and the mixture was extracted with ethyl acetate. The organic layer was washed with saturatedsaline, dried over anhydrous sodium sulfate, and then the solvent was removed under reduced pressure. The residuewas extracted with ethyl acetate-hexane (1:9) (700 mL), and the extract was stirred at room temperature for 3 hours.Insolubles were collected by filtration, washed with hexane, and dried to afford the title compound (49.2 g). For thefiltrate, the solvent was removed under the reduced pressure, and the residue was purified by silica gel column chromatographyto afford the title compound (15.9 g).

References: [1]Bioorganic and Medicinal Chemistry Letters,1999,vol. 9,p. 369 - 374.
[2]Patent: EP3792260,2021,A1 .Location in patent: Paragraph 0329.

4
[ 2239-31-8 ]
[ 36176-31-5 ]
C₁₇H₂₆N₂OS [ No CAS ]