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Chemical Structure| 214360-74-4 Chemical Structure| 214360-74-4
Chemical Structure| 214360-74-4

2-(3-(Bromomethyl)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

CAS No.: 214360-74-4

4.5 *For Research Use Only !

Cat. No.: A760029 Purity: 98%

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Product Details of [ 214360-74-4 ]

CAS No. :214360-74-4
Formula : C13H18BBrO2
M.W : 297.00
SMILES Code : BrCC1=CC(B(OC2(C)C)OC2(C)C)=CC=C1
MDL No. :MFCD02183481
InChI Key :WUIYGXGXVOHAFW-UHFFFAOYSA-N
Pubchem ID :2773283

Safety of [ 214360-74-4 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302+H312-H314
Precautionary Statements:P260-P264-P270-P280-P301+P312+P330-P301+P330+P331-P303+P361+P353-P304+P340+P310-P305+P351+P338+P310-P362+P364-P405-P501
Class:8
UN#:3261
Packing Group:

Application In Synthesis of [ 214360-74-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 214360-74-4 ]

[ 214360-74-4 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 110-91-8 ]
  • [ 214360-74-4 ]
  • [ 364794-80-9 ]
  • 2
  • [ 76-09-5 ]
  • [ 51323-43-4 ]
  • [ 214360-74-4 ]
YieldReaction ConditionsOperation in experiment
4.43 g With magnesium sulfate; In ethyl acetate; at 20℃; for 8h; To a solution of <strong>[51323-43-4]3-(bromomethyl)phenyl boronic acid</strong> (3.13 g) in ethyl acetate (45 ml) were sequentially added pinacol (1.72 g) and anhydrous magnesium sulfate (15 g) at room temperature, and the mixture was stirred for 8 hours. The insoluble substance was filtered off, and the filtrate was concentrated under reduced pressure to give the titled compound (4.43 g). 1H-NMR (CDCl3) delta: 1.33 (s, 12H), 4.49 (s, 2H), 7.31-7.37 (m, 1H), 7.46-7.50 (m, 1H), 7.70-7.74 (m, 1H), 7.79-7.82 (m, 1H).
 

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[ 214360-74-4 ]

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