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Structure of 17536-00-4

Chemical Structure| 17536-00-4

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Product Details of [ 17536-00-4 ]

CAS No. :17536-00-4
Formula : C9H16N2
M.W : 152.24
SMILES Code : CC(C1=CC(C(C)C)=NN1)C
MDL No. :MFCD00671516
InChI Key :PJSJVTZSFIRYIZ-UHFFFAOYSA-N
Pubchem ID :5255229

Safety of [ 17536-00-4 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319
Precautionary Statements:P264-P280-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313

Application In Synthesis of [ 17536-00-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 17536-00-4 ]

[ 17536-00-4 ] Synthesis Path-Downstream   1~5

  • 1
  • [ 18362-64-6 ]
  • [ 17536-00-4 ]
YieldReaction ConditionsOperation in experiment
100% With hydrazine; In ethanol; at 20℃; for 2h; Hydrazine (330 mg, 10 mmol) was added to a solution of 2,6-dimethylheptane-3,5- dione (1.6 g, 10 mmol) in ethanol (40 mL) at room temperature. After 2 hours, the reaction was concentrated in vacuo to afford 3, 5-diisopropyl-lH-pyrazole (1.5 g, 10 mmol, yield: 100%) which was used in the next step without further purification. MS: m/z 153.1 (M+H+).
  • 2
  • manganese(II) chloride tetrahydrate [ No CAS ]
  • [ 3847-57-2 ]
  • [ 17536-00-4 ]
  • [ 921933-07-5 ]
  • 3
  • cobalt(II) nitrate hexahydrate [ No CAS ]
  • [ 3847-57-2 ]
  • [ 17536-00-4 ]
  • [ 945734-41-8 ]
  • 4
  • [ 7089-68-1 ]
  • [ 17536-00-4 ]
  • [ 1428871-22-0 ]
YieldReaction ConditionsOperation in experiment
75.8% under nitrogen conditions, to a stirred solution has 0.76g (50mmol) 50ml dimethylformamide, 3,5-diisopropyl-pyrazole (DMF) was added 0.12g (50mmol) of sodium hydride, stirred for a few minutes, then was slowly added 1.07g (50mmol) 2- chloro-1,10-phenanthroline, the reaction was refluxed for 72h, cooled, cold water, the white precipitate was filtered off, and then recrystallized with ethanol to give white crystals of 2- (3 , 5-isopropyl-pyrazol) 1,10-phenanthroline, a yield of 75.8percent.
  • 5
  • [ 7089-68-1 ]
  • [ 17536-00-4 ]
  • [ 1451010-45-9 ]
 

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