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Chemical Structure| 17135-78-3 Chemical Structure| 17135-78-3

Structure of 17135-78-3

Chemical Structure| 17135-78-3

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Product Details of [ 17135-78-3 ]

CAS No. :17135-78-3
Formula : C14H9Cl
M.W : 212.67
SMILES Code : ClC1=CC2=CC3=CC=CC=C3C=C2C=C1
MDL No. :MFCD00003580
InChI Key :OWFINXQLBMJDJQ-UHFFFAOYSA-N
Pubchem ID :28308

Safety of [ 17135-78-3 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319
Precautionary Statements:P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313

Application In Synthesis of [ 17135-78-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 17135-78-3 ]

[ 17135-78-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 17135-78-3 ]
  • [ 15424-38-1 ]
  • C34H23N [ No CAS ]
YieldReaction ConditionsOperation in experiment
85% With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate; In toluene; for 2h;Reflux; Tri-tert-butylphosphine (3 mL of a 1.0 M solution in toluene, 7.32 mmol), palladium acetate (0.4 g, 1.83 mmol) and sodium tert- butoxide (52.7 g, 549 mmol) were added to 2- chloroanthracene ) And Intermediate A-1 (49.2 g, 183 mmol) in degassed toluene (500 mL) and the mixture was heated at reflux for 2 h. The reaction mixture was cooled to room temperature, diluted with toluene and filtered through celite. The filtrate was diluted with water and extracted with toluene, and the organic phases were combined and evaporated under vacuum. The residue is filtered through silica gel and recrystallized to give the target product TM1 (69.2 g, 85% yield).
 

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