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Chemical Structure| 14204-24-1 Chemical Structure| 14204-24-1

Structure of 14204-24-1

Chemical Structure| 14204-24-1

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Product Details of [ 14204-24-1 ]

CAS No. :14204-24-1
Formula : C10H9NO2S
M.W : 207.25
SMILES Code : O=C(CC1)N(SC2=CC=CC=C2)C1=O
MDL No. :N/A

Safety of [ 14204-24-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 14204-24-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 14204-24-1 ]

[ 14204-24-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 14204-24-1 ]
  • [ 14752-66-0 ]
  • [ 1142-97-8 ]
YieldReaction ConditionsOperation in experiment
72% With scandium tris(trifluoromethanesulfonate); In water; at 30℃; for 6h;Ionic liquid; General procedure: To a solution of 1 (0.3 mmol) and 2 (0.36 mmol) in [BMIM]PF6 (3 mL) and H2O (1 mL), Sc(OTf)3 was added at 30 C. The mixture solution was stirred at 30 C for respective time. After the completion of the reaction, as monitored by TLC and GC-MS analysis, the mixture was washed with water and extracted with diethyl ether. The organic phase was concentrated and the resulting residue was purified by column chromatography on silica gel (300-400 mesh) with petroleum ether-EtOAc as eluent to provide the desired thiosulfonates 3.
 

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