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Chemical Structure| 14092-11-6 Chemical Structure| 14092-11-6

Structure of 14092-11-6

Chemical Structure| 14092-11-6

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Product Details of [ 14092-11-6 ]

CAS No. :14092-11-6
Formula : C11H19N
M.W : 165.28
SMILES Code : N1(C2=CCCCCC2)CCCC1

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Application In Synthesis of [ 14092-11-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 14092-11-6 ]

[ 14092-11-6 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 14092-11-6 ]
  • [ 114078-88-5 ]
  • [ 51490-23-4 ]
YieldReaction ConditionsOperation in experiment
67% In chloroform; at 0 - 45℃; for 0.75h;Molecular sieve; Compound (M-21) (2.00 g, 12.5 mmol) was dissolved in chloroform (25.0 mL), 4A molecular sieve (400 mg,powder) was added, compound (M-22) (3.10 g, 18.8 mmol) was added at 0C, and the mixture was stirred at 0C for 5min. After stirring at 45C for 40 min, the mixture was allowed to cool to room temperature. The solvent was evaporatedunder reduced pressure, and the residue was purified by silica gel column chromatography (n-hexane:ethyl acetate) togive compound (M-23) (yield 1.90 g, 67%)
  • 2
  • [ 14092-11-6 ]
  • [ 114078-88-5 ]
  • C10H12BrN [ No CAS ]
YieldReaction ConditionsOperation in experiment
67% In chloroform; at 0 - 45℃; for 0.75h;Molecular sieve; Compound (M-21) (2.00 g, 12.5 mmol)Was dissolved in chloroform (25.0 mL)4 A molecular sieve (400 mg, powder)And the compound (M-22) (3.10 g, 18.8 mmol) was added at 0 C.,And the mixture was stirred at 0 C. for 5 minutes.After stirring at 45 C. for 40 minutes, it was allowed to cool to room temperature.The solvent was distilled off under reduced pressure,The residue was purified by silica gel column chromatography (n-hexane: ethyl acetate)Compound (M-23)(Yield 1.90 g, yield 67%).
 

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