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Chemical Structure| 126989-14-8 Chemical Structure| 126989-14-8

Structure of 126989-14-8

Chemical Structure| 126989-14-8

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Product Details of [ 126989-14-8 ]

CAS No. :126989-14-8
Formula : C21H27NO10
M.W : 453.44
SMILES Code : O=C(C(C(OCC)=O)C(C1=CC=C([N+]([O-])=O)C=C1)C(C(OCC)=O)C(OCC)=O)OCC

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Application In Synthesis of [ 126989-14-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 126989-14-8 ]

[ 126989-14-8 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 126989-14-8 ]
  • [ 92289-14-0 ]
YieldReaction ConditionsOperation in experiment
88% With hydrogenchloride; water; at 100℃; for 22h;Product distribution / selectivity; g) 3-(4-Nitro-phenyl)-pentanedioic acid A suspension of 7.32 g (16.1 mmol) of 2,4-bis-ethoxycarbonyl-3-(4-nitro-phenyl)-pentanedioic acid diethyl ester (as prepared in the previous step) in concentrated HCl (15 mL) was heated to 100 C. for 22 h. The mixture was cooled to RT, and the resulting precipitate was filtered, washed with cold water, and air-dried to afford 3.58 g (88%) of the title compound as an off-white solid: 1H-NMR (CD3OD; 400 MHz): δ 8.12 (d, 2H, J=8.8 Hz), 7.58 (d, 2H, J=8.8 Hz), 3.77-3.68 (m, 1H), 2.87-2.66 (m, 4H).
  • 2
  • [ 7647-01-0 ]
  • [ 126989-14-8 ]
  • [ 92289-14-0 ]
 

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