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Chemical Structure| 121-63-1 Chemical Structure| 121-63-1

Structure of 121-63-1

Chemical Structure| 121-63-1

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Product Details of [ 121-63-1 ]

CAS No. :121-63-1
Formula : C12H8Cl2O5S2
M.W : 367.22
SMILES Code : O=S(C1=CC=C(OC2=CC=C(S(=O)(Cl)=O)C=C2)C=C1)(Cl)=O
MDL No. :MFCD00024884
InChI Key :HJKXLQIPODSWMB-UHFFFAOYSA-N
Pubchem ID :8484

Safety of [ 121-63-1 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H290-H314
Precautionary Statements:P234-P260-P264-P280-P301+P330+P331+P310-P303+P361+P353+P310+P363-P304+P340+P310-P305+P351+P338+P310-P390-P405-P406-P501
Class:8
UN#:3261
Packing Group:

Application In Synthesis of [ 121-63-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 121-63-1 ]

[ 121-63-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 121-63-1 ]
  • [ 53786-10-0 ]
  • C38H40N6O7S2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With triethylamine; In tetrahydrofuran; dichloromethane; at 20℃; A solution of l,3-dihydro-l-methyl-3-(4-piperidinyl)-2//-benzimidazol-2-one (0.0005 mol) in dichloromethane (2 ml) was mixed with a solution of JV, JV-diethylethanamine (0.0006 mol) in dichloromethane (1 ml). This mixture was treated dropwise with a solution of 4,4'-oxybisbenzenesulfonyl chloride (0.00025 mol) in THF (1 ml) and the resulting reaction mixture was stirred overnight under atmospheric conditions. The desired compound was isolated and purified by high-performance liquid chromatography over Kromasil Spherical underivated silica gel (55 g, 60 A, 5 um; eluent: CHaCl^OH^yCKbOH 9/l)/CH3OH. The desired fractions were collected and the solvent was evaporated, yielding 0.140 g of compound 4.
 

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