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Chemical Structure| 111088-69-8 Chemical Structure| 111088-69-8

Structure of 111088-69-8

Chemical Structure| 111088-69-8

(3-Methoxypropyl)triphenylphosphonium bromide

CAS No.: 111088-69-8

4.5 *For Research Use Only !

Cat. No.: A326255 Purity: 95%

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Product Details of [ 111088-69-8 ]

CAS No. :111088-69-8
Formula : C22H24BrOP
M.W : 415.30
SMILES Code : [Br-].COCCC[P+](C1=CC=CC=C1)(C1=CC=CC=C1)C1=CC=CC=C1
MDL No. :MFCD20482687
InChI Key :LHNDMMYQNGTXEA-UHFFFAOYSA-M
Pubchem ID :21458797

Safety of [ 111088-69-8 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302+H312-H315-H319
Precautionary Statements:P501-P270-P264-P280-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330-P302+P352+P312

Application In Synthesis of [ 111088-69-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 111088-69-8 ]

[ 111088-69-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 103058-87-3 ]
  • [ 111088-69-8 ]
  • [ 865156-70-3 ]
YieldReaction ConditionsOperation in experiment
a) 5-Bromo-2-methoxv-3- (4-methoxv-but-1 (E, Z)-envl)-pvridine; 2. 45 ml of a 1M solution of sodium-bis(trimethylsilyl) amide in tetrahydrofuran are added. to a suspension of 2. 4 mmol (3-methoxy-propyl)-triphenyl-phosphonium bromide [111088-69-8] in 8 mi tetrahydrofuran unter an argon atmosphere at 0C. The reaction mixture is stirred for 30 minutes at 0C and then 1. 6 mmol <strong>[103058-87-3]5-bromo-2-methoxy-pyridine-3-carbaldehyde</strong> [103058-87- 3] are added. The reaction mixture is warmed to room temperature and then diluted with tert- butyl methyl ether. The solution is washed with saturated aqueous sodium hydrogencarbonate solution. The organic layer is dried over sodium sulphate, filtered and concentrated. The title compound is obtained from the residue by means of flash chromatography (SiO2 60F) and identified based on its Rf value
 

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