Home Cart Sign in  
Chemical Structure| 256-96-2 Chemical Structure| 256-96-2
Chemical Structure| 256-96-2

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

Iminostilbene (Dibenzazepine) is a chemical precursor of carbamazepine which is used primarily in the treatment of epilepsy and neuropathic pain.

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of Iminostilbene

CAS No. :256-96-2
Formula : C14H11N
M.W : 193.24
SMILES Code : C12=CC=CC=C1C=CC3=CC=CC=C3N2
MDL No. :MFCD00005071
InChI Key :LCGTWRLJTMHIQZ-UHFFFAOYSA-N
Pubchem ID :9212

Safety of Iminostilbene

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of Iminostilbene

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 256-96-2 ]

[ 256-96-2 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 256-96-2 ]
  • [ 105-40-8 ]
  • [ 41359-02-8 ]
  • 2
  • [ 256-96-2 ]
  • [ 155613-52-8 ]
  • [ 1265884-98-7 ]
  • 4
  • [ 256-96-2 ]
  • [ 57103-20-5 ]
  • 5-5’-(9-phenyl-9H-carbazol-3,6-diyl)bis(5H-dibenzo[b,f]azepine) [ No CAS ]
YieldReaction ConditionsOperation in experiment
73.3% With copper; potassium carbonate; In 1-methyl-pyrrolidin-2-one; for 48h;Reflux; Inert atmosphere; Under nitrogen protection,Intermediate A-1 (40.1 g, 0.1 mol) and iminopil (48.3 g, 0.25 mol) were dissolved in500 mL of NMP (N-methylpyrrolidone)Then, a catalyst copper powder (19.1 g, 0.3 mol) and an acid binding agent potassium carbonate were charged(55.3 g, 0.4 mol).The system was heated to reflux for 48 hours,Natural cooling to 20 ~ 25 after adding 1000mL of water quenchedReaction, the product is filtered to obtain crude.Silica gel column chromatography, eluting with dichloromethane: n-hexane = 1: 7 (v / v)White powder.Further crude product was purified by sublimation in a chemical vapor deposition system at 320 ° C to obtain 45.9 g of an off-white solid powder,The yield was 73.3percent.
 

Historical Records

Technical Information

Categories