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Chemical Structure| 97973-95-0 Chemical Structure| 97973-95-0

Structure of 97973-95-0

Chemical Structure| 97973-95-0

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Product Details of [ 97973-95-0 ]

CAS No. :97973-95-0
Formula : C10H15NO3
M.W : 197.23
SMILES Code : O=C(OC(C)(C)C)N[C@H](C(C#C)=O)C

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Application In Synthesis of [ 97973-95-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 97973-95-0 ]

[ 97973-95-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 97973-95-0 ]
  • [ 29097-00-5 ]
  • methyl (1′S)-7-{1-[(tert-butoxycarbonyl)amino]ethyl}pyrazolo[1,5-a]pyrimidine-3-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
70% With acetic acid; In methanol; water; at 20℃; for 168h; General procedure: A solution of 5-aminopyrazole 5g (1 mmol) and ynone 7 (1 mmol) inMeOH (1 mL) was added dropwise to a mixture of AcOH (0.5 mL) andwater (10 mL) and the mixture was stirred at r.t. for 7 days. The productwas extracted by CH2Cl2 (3×25 mL) and the combined organic phaseswere dried over anhydrous Na2SO4, filtered, and the filtrate was evaporatedin vacuo. The residue was purified by CC (EtOAc/hexanes).Fractions containing the product were combined and evaporated invacuo to give 10.
 

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