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Chemical Structure| 97776-06-2 Chemical Structure| 97776-06-2

Structure of 97776-06-2

Chemical Structure| 97776-06-2

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Product Details of [ 97776-06-2 ]

CAS No. :97776-06-2
Formula : C8H8INO
M.W : 261.06
SMILES Code : CC(C1=CC=C(N)C(I)=C1)=O
MDL No. :MFCD22124432

Safety of [ 97776-06-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis of [ 97776-06-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 97776-06-2 ]

[ 97776-06-2 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 544-92-3 ]
  • [ 97776-06-2 ]
  • [ 33720-71-7 ]
YieldReaction ConditionsOperation in experiment
56.9% In DMF (N,N-dimethyl-formamide); for 6.0h;Heating / reflux; b.. Preparation of 3-cyano-4-amino-acetophenone The 3-iodo-4-amino-acetophenone as prepared above was dissolved 95ml of DMF and 20.9g CuCN was added.. Stirred under reflux for 6h and cooled down to 100C. The reaction mixture was poured into 2L of water, and cooled.. The precipitate was filtered off, air dried and extracted with THF. Evaporated, washed with ethanol, filtered, and dried to give product as yellow crystal.. Yield 56.9%; melting point 150-152C.
  • 2
  • [ 557-21-1 ]
  • [ 97776-06-2 ]
  • [ 33720-71-7 ]
 

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Technical Information

• Alkyl Halide Occurrence • Baeyer-Villiger Oxidation • Barbier Coupling Reaction • Baylis-Hillman Reaction • Bucherer-Bergs Reaction • Buchwald-Hartwig C-N Bond and C-O Bond Formation Reactions • Chan-Lam Coupling Reaction • Clemmensen Reduction • Corey-Bakshi-Shibata (CBS) Reduction • Corey-Chaykovsky Reaction • Fischer Indole Synthesis • General Reactivity • Grignard Reaction • Henry Nitroaldol Reaction • Hiyama Cross-Coupling Reaction • Horner-Wadsworth-Emmons Reaction • Hydride Reductions • Kinetics of Alkyl Halides • Lawesson's Reagent • Leuckart-Wallach Reaction • Mannich Reaction • McMurry Coupling • Meerwein-Ponndorf-Verley Reduction • Passerini Reaction • Paternò-Büchi Reaction • Petasis Reaction • Peterson Olefination • Pictet-Spengler Tetrahydroisoquinoline Synthesis • Preparation of Aldehydes and Ketones • Preparation of Amines • Prins Reaction • Reactions of Aldehydes and Ketones • Reactions of Alkyl Halides with Reducing Metals • Reactions of Amines • Reactions of Benzene and Substituted Benzenes • Reactions of Dihalides • Reformatsky Reaction • Robinson Annulation • Schlosser Modification of the Wittig Reaction • Schmidt Reaction • Specialized Acylation Reagents-Ketenes • Specialized Acylation Reagents-Vilsmeier Reagent • Stobbe Condensation • Substitution and Elimination Reactions of Alkyl Halides • Suzuki Coupling • Tebbe Olefination • Ugi Reaction • Wittig Reaction • Wolff-Kishner Reduction

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