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Chemical Structure| 97271-97-1 Chemical Structure| 97271-97-1

Structure of 97271-97-1

Chemical Structure| 97271-97-1

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Product Details of [ 97271-97-1 ]

CAS No. :97271-97-1
Formula : C7H6N2O3
M.W : 166.13
SMILES Code : NC1=C(C=O)C=CC=C1[N+]([O-])=O
MDL No. :MFCD09880173
InChI Key :LDKGAMZVANIDGZ-UHFFFAOYSA-N
Pubchem ID :13419753

Safety of [ 97271-97-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 97271-97-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 97271-97-1 ]

[ 97271-97-1 ] Synthesis Path-Downstream   1~7

  • 1
  • [ 607-35-2 ]
  • [ 64-19-7 ]
  • [ 25369-31-7 ]
  • [ 606-18-8 ]
  • [ 97271-98-2 ]
  • [ 97272-30-5 ]
  • [ 97271-96-0 ]
  • [ 97271-97-1 ]
  • 2
  • [ 97271-97-1 ]
  • [ 3442-60-2 ]
  • [ 1403215-47-3 ]
YieldReaction ConditionsOperation in experiment
72% With methanesulfonic acid; In ethanol; for 25.5h;Inert atmosphere; Reflux; 5.1.143 8'-Amino-6,7-didehydro-3-methoxy-17-methylquinolino[2',3':6,7]morphinan-14beta-ol (32d) Compound 32d was prepared from compound 23d according to the procedure used to prepare compound 32a. Yield, 36%; a yellow amorphous solid. IR (KBr): 3437, 2930, 1592, 1497, 1273, 1044 cm-1. 1H NMR (300 MHz, CDCl3) delta: 1.35-1.46 (1H, m), 2.19-2.31 (2H, m), 2.41-2.48 (1H, m), 2.44 (3H, s), 2.88-3.08 (4H, m), 3.25 (1H, d, J = 18.3 Hz), 3.54 (1H, d, J = 17.4 Hz), 3.64 (3H, s), 3.67 (1H, d, J = 17.4 Hz), 4.63 (1H, br s), 6.60 (1H, dd, J = 2.7, 8.4 Hz), 6.80 (1H, dd, J = 1.2, 7.5 Hz), 6.90 (1H, d, J = 2.4 Hz), 6.94 (1H, dd, J = 1.2, 8.1 Hz), 7.00 (1H, d, J = 8.4 Hz), 7.16 (1H, t, J = 7.8 Hz), 7.55 (1H, s), two protons (NH2) were not observed. 13C NMR (75 MHz, CDCl3) delta: 24.0, 36.0, 36.6, 39.3, 40.5, 42.9, 45.6, 55.0, 61.8, 69.5, 109.0, 111.4, 111.5, 115.3, 126.0, 127.5, 127.6, 128.1, 128.3, 135.0, 136.9, 141.3, 143.1, 154.3, 158.1. HRMS (ESI) Calcd for C25H28N3O2 [M+H]+: 402.2182. Found: 402.2180.
  • 3
  • [ 139743-08-1 ]
  • [ 97271-97-1 ]
YieldReaction ConditionsOperation in experiment
78% With manganese(IV) oxide; In Dichlorodifluoromethane; at 20.0℃; for 23.0h;Inert atmosphere; 5.1.142 6,7-Didehydro-17-methyl-8'-nitroquinolino[2',3':6,7]morphinan-3,14beta-diol hydrochloride (SYK-349) SYK-349 was prepared from compound 29d according to the procedure used to prepare SYK-27. Yield, 98%; a brown amorphous solid. Mp 255-262 C (dec). Anal. Calcd for C24H23N3O4·1.5HCl·0.5H2O: C, 59.91; H, 5.34; N, 8.73. Found: C, 60.10; H, 5.42; N, 8.46.
  • 4
  • [ 97271-97-1 ]
  • [ 1403215-51-9 ]
  • 5
  • [ 97271-97-1 ]
  • C24H23N3O4*ClH [ No CAS ]
  • 6
  • [ 97271-97-1 ]
  • [ 1403215-55-3 ]
  • 7
  • [ 180995-26-0 ]
  • [ 97271-97-1 ]
  • 2-((4aS,5R,10bR)-7-nitro-3,4,4a,5,6,10b-hexahydro-2H-pyrano[3,2-c]quinolin-5-yl)phenol [ No CAS ]
 

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Technical Information

• Barbier Coupling Reaction • Baylis-Hillman Reaction • Benzylic Oxidation • Birch Reduction • Blanc Chloromethylation • Bucherer-Bergs Reaction • Buchwald-Hartwig C-N Bond and C-O Bond Formation Reactions • Chan-Lam Coupling Reaction • Clemmensen Reduction • Complex Metal Hydride Reductions • Corey-Chaykovsky Reaction • Corey-Fuchs Reaction • Fischer Indole Synthesis • Friedel-Crafts Reaction • Grignard Reaction • Hantzsch Dihydropyridine Synthesis • Henry Nitroaldol Reaction • Horner-Wadsworth-Emmons Reaction • Hydride Reductions • Hydrogenolysis of Benzyl Ether • Julia-Kocienski Olefination • Knoevenagel Condensation • Leuckart-Wallach Reaction • Mannich Reaction • McMurry Coupling • Meerwein-Ponndorf-Verley Reduction • Mukaiyama Aldol Reaction • Nozaki-Hiyama-Kishi Reaction • Passerini Reaction • Paternò-Büchi Reaction • Petasis Reaction • Pictet-Spengler Tetrahydroisoquinoline Synthesis • Preparation of Aldehydes and Ketones • Preparation of Alkylbenzene • Preparation of Amines • Prins Reaction • Reactions of Aldehydes and Ketones • Reactions of Amines • Reactions of Benzene and Substituted Benzenes • Reformatsky Reaction • Schlosser Modification of the Wittig Reaction • Schmidt Reaction • Specialized Acylation Reagents-Vilsmeier Reagent • Stetter Reaction • Stobbe Condensation • Tebbe Olefination • Ugi Reaction • Vilsmeier-Haack Reaction • Wittig Reaction • Wolff-Kishner Reduction

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