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Chemical Structure| 943323-35-1 Chemical Structure| 943323-35-1

Structure of 943323-35-1

Chemical Structure| 943323-35-1

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Product Details of [ 943323-35-1 ]

CAS No. :943323-35-1
Formula : C14H22N2O2
M.W : 250.34
SMILES Code : O=C(OC(C)(C)C)NCC(N)CC1=CC=CC=C1
MDL No. :MFCD11858346
InChI Key :ADVSLLRGGNVROC-UHFFFAOYSA-N
Pubchem ID :20159911

Safety of [ 943323-35-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis of [ 943323-35-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 943323-35-1 ]

[ 943323-35-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 943323-35-1 ]
  • [ 1246616-66-9 ]
  • [ 1246617-09-3 ]
YieldReaction ConditionsOperation in experiment
In toluene; at 100℃; for 2.5h; Fourth StepDimethyl 3-(benzyloxy)-4-oxo-4H-pyran-2,5-dicarboxylate (313 mg, 0.983 mmol) and 28D (246 mg, 0.983 mmol) were added to toluene (3 ml), and the mixture was stirred at 100 C. for 2.5 hours. After the solvent was distilled off under reduced pressure, the resulting crude product was purified by silica gel column chromatography (chloroform-methanol, 98.2, v/v) to obtain 320 mg of Compound 28E as a pale yellow gummy substance.1H-NMR (CDCl3) delta: 1.42 (9H, s), 3.07 (2H, m), 3.56 (2H, m), 3.68 (3H, s), 3.95 (3H, s), 4.26 (1H, s), 4.86 (1H, s), 5.18 (1H, d, J=10.8 Hz), 5.22 (1H, d, J=10.8 Hz), 7.01 (2H, m), 7.24-7.38 (8H, m), 8.22 (1H, s).MS: m/z=551 [M+H]+.
 

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