Home Cart Sign in  
Chemical Structure| 939979-32-5 Chemical Structure| 939979-32-5

Structure of 939979-32-5

Chemical Structure| 939979-32-5

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 939979-32-5 ]

CAS No. :939979-32-5
Formula : C6H4Cl2N4
M.W : 203.03
SMILES Code : CN1N=CC2=NC(Cl)=NC(Cl)=C21
MDL No. :MFCD14584722
InChI Key :ILSHTSRLVMUZKS-UHFFFAOYSA-N
Pubchem ID :57415862

Safety of [ 939979-32-5 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 939979-32-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 939979-32-5 ]

[ 939979-32-5 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 939979-32-5 ]
  • [ 1228947-14-5 ]
  • C16H22ClN5O2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
75% <strong>[1228947-14-5](1r,4r)-<strong>[1228947-14-5]4-(morpholin-4-yl)cyclohexan-1-ol</strong></strong> (201 mg, 1.08 mmol, 1.10 eq.) was placed into a 25-mL 3-necked round-bottom flask and dissolved in THF (1 mL). The reaction was cooled to at 0 C and LiHMDS-THF (1 mL, 1.10 eq.) was added dropwise. The resulting solution was stirred for 15 min at room temperature and then compound 1.1 (200 mg, 0.99 mmol, 1.00 eq.) was added. The reaction was stirred for 1 h at room temperature. Upon completion, the mixture was concentrated in vacuo and diluted with water and CH2CI2. The resulting solution was extracted with 3 x 10 mL of CH2CI2, and the organic layers were combined, dried over anhydrous Na2S04 and concentrated in vacuo. Crude material was purified by column chromatography to furnish 260 mg (75%) of compound 4.1 as yellow oil.
  • 2
  • [ 939979-32-5 ]
  • [ 1228947-14-5 ]
  • 1-methyl-N-(1-methyl-1H-pyrazol-4-yl)-7-(((1r,4r)-4-morpholinocyclohexyl)oxy)-1H-pyrazolo[4,3-d]pyrimidin-5-amine [ No CAS ]
  • 3
  • [ 939979-32-5 ]
  • [ 114474-28-1 ]
  • N-(4-(1H-pyrazol-4-yl)phenyl)-5-chloro-1-methyl-1H-pyrazolo[4,3-d]pyrimidin-7-amine [ No CAS ]
YieldReaction ConditionsOperation in experiment
97% With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 100.0℃; for 5.0h; [0244] A mixture of 5,7-dichloro-l-methyl-lH-pyrazolo[4,3-d]pyrimidine (300 mg, 1.50 mmol), 4-(lH-pyrazol-4-yl)aniline (235, 1.50 mmol), and iPr2NEt (0.52 mL, 0.74 mmol) in DMF (3.0 mL) was heated at 100 C for 5h, cooled to rt, and diluted with water. The precipitate formed was collected by filtration and washed with water and dried in vacuo to provide the title compound (465 mg, 97%). MS(ES+) m/e 326 (M+H)+.
 

Historical Records

Technical Information

Categories