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Chemical Structure| 939791-42-1 Chemical Structure| 939791-42-1

Structure of 939791-42-1

Chemical Structure| 939791-42-1

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Product Details of [ 939791-42-1 ]

CAS No. :939791-42-1
Formula : C8H13N3O2S
M.W : 215.27
SMILES Code : CN(C1=NC=CC=C1CN)S(C)(=O)=O
MDL No. :MFCD15071408

Safety of [ 939791-42-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 939791-42-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 939791-42-1 ]

[ 939791-42-1 ] Synthesis Path-Downstream   1~5

  • 1
  • [ 6625-94-1 ]
  • [ 939791-42-1 ]
  • C16H15Cl2N5O2S [ No CAS ]
YieldReaction ConditionsOperation in experiment
70.3% With triethylamine; In dichloromethane; at 20℃; for 4h; 297 mg (1.28 mmol) of compound A-3,275 mg (1.28 mmol) of compound N- (3- (aminomethyl) pyridin-2-yl) -N-methylmethanesulfonamide and0.356 mL (2.56 mmol) of triethylamine was dissolved in 15 mL of dichloromethane,Stir at room temperature.After 4 h reaction,The solvent was distilled off under reduced pressure, and the resulting crude product was washed with diethyl ether,A white solid B-3 was obtained in a yield of 70.3%.
  • 2
  • [ 6625-94-1 ]
  • [ 939791-42-1 ]
  • C24H22ClN7O3S [ No CAS ]
  • 3
  • [ 939791-42-1 ]
  • [ 62484-29-1 ]
  • C16H15Cl2N5O2S [ No CAS ]
YieldReaction ConditionsOperation in experiment
68.9% With triethylamine; In dichloromethane; at 20℃; for 4h; 297 mg (1.28 mmol) of compound A-4,275 mg (1.28 mmol) of compound N- (3- (aminomethyl) pyridin-2-yl) -N-methylmethanesulfonamide and0.356 mL (2.56 mmol) of triethylamine was dissolved in 15 mL of dichloromethane,Stir at room temperature.After 4 h reaction,The solvent was distilled off under reduced pressure, and the resulting crude product was washed with diethyl ether,A white solid B-4 was obtained in a yield of 68.9%.
  • 4
  • [ 87611-00-5 ]
  • [ 939791-42-1 ]
  • C16H15ClFN5O2S [ No CAS ]
YieldReaction ConditionsOperation in experiment
52.8% With triethylamine; In dichloromethane; at 20℃; for 4.0h; 300 mg (1.38 mmol) of compound A-5,297 mg (1.38 mmol) of compound N- (3- (aminomethyl) pyridin-2-yl) -N-methylmethanesulfonamide and0.4 mL of triethylamine was dissolved in 15 mL of dichloromethane,Stir at room temperature.After 4 h reaction,The solvent was distilled off under reduced pressure, and the resulting crude product was washed with diethyl ether,To give an off-white solid B-5 in a yield of 49.0%.
  • 5
  • [ 87611-00-5 ]
  • [ 939791-42-1 ]
  • C24H22FN7O3S [ No CAS ]
 

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