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Chemical Structure| 939027-86-8 Chemical Structure| 939027-86-8

Structure of 939027-86-8

Chemical Structure| 939027-86-8

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Product Details of [ 939027-86-8 ]

CAS No. :939027-86-8
Formula : C5H12N2O
M.W : 116.16
SMILES Code : O=CNNC(C)CC

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Application In Synthesis of [ 939027-86-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 939027-86-8 ]

[ 939027-86-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 939027-86-8 ]
  • [ 184177-81-9 ]
  • [ 106461-41-0 ]
YieldReaction ConditionsOperation in experiment
61.1% With N-ethyl-N,N-diisopropylamine; In 5,5-dimethyl-1,3-cyclohexadiene; at 140℃; for 20h; 20.0 g of Compound 3 (0.051 mol) (R = phenyl) and 5.9 g of Compound 4 (0.051 mol) were sequentially added to a 500 ml three-necked flask.7.8 g of N,N-diisopropylethylamine (0.06 mol), 200 ml of xylene,Warm to 140 C. The reaction was detected by TLC and the reaction was complete at 20 h. Heat off and cool to room temperature. After suction filtration, the cake was recrystallized from 180 ml of a mixed solvent (toluene: isopropyl alcohol = 1:1) to give 12.3 g of pale yellow solid.Purity >99.5%.
 

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