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Chemical Structure| 93884-11-8 Chemical Structure| 93884-11-8

Structure of 93884-11-8

Chemical Structure| 93884-11-8

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Product Details of [ 93884-11-8 ]

CAS No. :93884-11-8
Formula : C10H13NO4S
M.W : 243.28
SMILES Code : O=C(OCC)C1=CC=CC(NS(=O)(C)=O)=C1
MDL No. :MFCD02861886

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Application In Synthesis of [ 93884-11-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 93884-11-8 ]

[ 93884-11-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 93884-11-8 ]
  • [ 376347-09-0 ]
YieldReaction ConditionsOperation in experiment
90% With lithium aluminium tetrahydride; In tetrahydrofuran; at 20℃; for 1.0h; Compound 3 To a 300 ml solution of 28.85 g (0.0945 mol) of compound 2 in THF is carefully added 5.32 g (0.140 mmol) of lithium aluminium hydride and the mixture is stirred for about 1 hr at room temperature. To the reaction mixture was added ethyl acetate and water under ice-cooling to decompose the excess of reducing agents. It was then partitioned between ethyl acetate and 2N HCI. the organic layer is washed with water and a saline, dried over MGS04, filtered and concentrated under reduced pressure to obtain a crude product. Recrystallization from methylene chloride/ether gives 22.34 g (0.0848 mol ; yield, 90%) of compound 3.
 

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