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Chemical Structure| 933474-39-6 Chemical Structure| 933474-39-6

Structure of 933474-39-6

Chemical Structure| 933474-39-6

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Product Details of [ 933474-39-6 ]

CAS No. :933474-39-6
Formula : C20H21NO3
M.W : 323.39
SMILES Code : O=C(N1C=CC2=C1C=C(OCC3=CC=CC=C3)C=C2)OC(C)(C)C
MDL No. :MFCD09801032

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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 933474-39-6 ]

[ 933474-39-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 933474-39-6 ]
  • [ 957204-30-7 ]
YieldReaction ConditionsOperation in experiment
With hydrogen;5%-palladium/activated carbon; In ethanol; for 24.0h; 6-Benzyloxy-1-(tert-butoxycarbonyl)-1H-indole (1.43 g) was dissolved in ethanol (20 mL), and 5% Pd/C was added to the solution. The reaction mixture was subjected to catalytic hydrogenation with stirring for 1 day. The catalyst was removed by filtration, and the filtrate was concentrated. The residue was purified by silica gel flash column chromatography (Yamazen Hi-Flash L), to thereby yield the title compound (1.15 g). NMR (CDCl3) delta: 1.55(9H,s), 2.98(2H,t,J=8.8Hz), 3.97(2H,t,J=8.3Hz),5.20-5.71(1H,m), 6.43(1H,dd,J=8.1,2.2Hz), 6.96(1H,d,J=8.5Hz), 7.55-7.34(1H,m). MS (ESI) m/z : 236 (M+H)+.
 

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