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Chemical Structure| 932-88-7 Chemical Structure| 932-88-7

Structure of 932-88-7

Chemical Structure| 932-88-7

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Product Details of [ 932-88-7 ]

CAS No. :932-88-7
Formula : C8H5I
M.W : 228.03
SMILES Code : IC#CC1=CC=CC=C1
MDL No. :MFCD00457145

Safety of [ 932-88-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H319-H332
Precautionary Statements:P261-P264-P271-P280-P304+P340+P312-P305+P351+P338

Application In Synthesis of [ 932-88-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 932-88-7 ]

[ 932-88-7 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 1116-77-4 ]
  • [ 932-88-7 ]
  • 4,4-diethoxy-N-methyl-N-(3-phenylprop-2-yn-1-yl)butan-1-amine [ No CAS ]
  • 2
  • [ 41042-12-0 ]
  • [ 932-88-7 ]
  • [ 1172590-88-3 ]
YieldReaction ConditionsOperation in experiment
89% With zinc; In tetrahydrofuran; for 4h;Reflux; General procedure: To a solution of N-substituted isatin (1 mmol) and iodoalkyne (1 mmol) in THF (3 mL) was added zinc dust (1 mmol), and the mixture was refluxed for completion of the reaction (TLC). The reaction mixture was cooled and filtered, and the filtrate was washed with saturated aq NH4Cl solution. The organic layer was concentrated and the residue was purified by column chromatography (ethyl acetate/hexane) to yield the pure product.
  • 3
  • [ 932-88-7 ]
  • [ 1195-33-1 ]
  • 1-bromo-4-((phenylethynyl)sulfonyl)benzene [ No CAS ]
YieldReaction ConditionsOperation in experiment
80% With air; In 1,2-dimethoxyethane; at 100℃; for 12h;Green chemistry; General procedure: To a mixture of alkynyliodine 1 (0.1 mmol), sulfinic acid 2 (0.2 mmol) in DME (2 mL) at room temperature under air. The reaction vessel was sealed and allowed to stir for 12 h at 100 C. After completion of the reaction, the resulting mixture was concentrated under vacuum and the residue was purified by flash column chromatography using a mixture of petroleum ether and ethyl acetate as eluent to give the desired products 3.
  • 4
  • [ 932-88-7 ]
  • [ 1388135-98-5 ]
  • [ 412947-54-7 ]
  • methyl (Z)-11-benzylidene-5-methyl-1-phenyl-2-tosyl-6,11-dihydro-2H-benzo[6,7]azepino[4,3,2-cd]indole-8-carboxylate [ No CAS ]
 

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