93107-30-3|1-Cyclopropyl-6,7-difluoro-4-oxo-1,4-dihydroquinoline-3-carboxylic acid| Ambeed

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Quality Control of [ 93107-30-3 ] Purity: 98% SDS Specification

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Product Details of [ 93107-30-3 ]

CAS No. :	93107-30-3
Formula :	C₁₃H₉F₂NO₃
M.W :	265.21
SMILES Code :	O=C(C1=CN(C2CC2)C3=C(C=C(F)C(F)=C3)C1=O)O
MDL No. :	MFCD01646375
InChI Key :	KNEXGVPHPGXAGF-UHFFFAOYSA-N
Pubchem ID :	5210422

Safety of [ 93107-30-3 ]

GHS Pictogram:
Signal Word:	Warning
Hazard Statements:	H302-H315-H319-H332-H335
Precautionary Statements:	P261-P280-P305+P351+P338

Application In Synthesis of [ 93107-30-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 93107-30-3 ]

[ 93107-30-3 ] Synthesis Path-Downstream 1~35

1
[ 503-29-7 ]
[ 93107-30-3 ]
1-cyclopropyl-6-fluoro-1,4-dihydro-7-[1'-azetidinyl]-4-oxo-3-quinoline-carboxylic acid [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
	With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile;	EXAMPLE 1 1-cyclopropyl-6-fluoro-1,4-dihydro-7-[1'-azetidinyl]-4-oxo-3-quinoline-carboxylic acid A mixture of 1-cyclopropyl-6,7-difluoro-1,4-dihydro-4-oxo-quinoline-3-carboxylic acid (1.591 g, 6 mmole), acetonitrile (70 ml), azetidine (390 mg, 6.8 mmole) and DBU (913 mg, 6 mmole) were heated at reflux. After only 5 minutes of heating, it was observed that crystalline material was precipitating. After 5 additional minutes of heating, the hot solution was filtered. The reaction mixture was then allowed to cool at room temperature for 1 hour. The solid material that precipitated was collected by filtration, washed first with acetonitrile and then with ethyl ether and then dried to give 650 mg of the title compound, m.p. 298°-299° C. (dec.). NMR(DMSO-D6): 1.12-1.13 d and 1.26-1.28 d, 4H of cyclopropane; 2.3-2.4, m, 2H of C3 'azetidine; 3.2-3.7, q, 1H of cyclopropane; 4.19-4.24, q, 4H of azetidine C2 ' and C4 '; 6.82- 6.85, d, 1H of C8; 7.74-7.78, d, 1H of C5; 8.55, s, 1H of C2.

References: [1]Journal of Medicinal Chemistry,1993,vol. 36,p. 801 - 810.
[2]Patent: US5039683,1991,A .

2
[ 110-85-0 ]
[ 93107-30-3 ]
[ 93107-08-5 ]

References: [1]Journal of Heterocyclic Chemistry,1987,vol. 24,p. 181 - 185.

3
[ 505-66-8 ]
[ 93107-30-3 ]
[ 118330-11-3 ]

References: [1]Journal of Medicinal Chemistry,1990,vol. 33,p. 142 - 146.

4
[ 90152-00-4 ]
[ 93107-30-3 ]
[ 118382-88-0 ]

References: [1]Journal of Medicinal Chemistry,1992,vol. 35,p. 611 - 620.

5
[ 5625-67-2 ]
[ 93107-30-3 ]
[ 103237-52-1 ]

References: [1]Arzneimittel-Forschung/Drug Research,1986,vol. 36,p. 1545 - 1549.

6
[ 45347-82-8 ]
[ 93107-30-3 ]
1-cyclopropyl-6-fluoro-1,4-dihydro-7-[3'-hydroxy-1'-azetidinyl]-4-oxo-3-quinolinecarboxylic acid [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1993,vol. 36,p. 801 - 810.

7
[ 127371-54-4 ]
[ 93107-30-3 ]

References: [1]Synthesis,2006,p. 963 - 968.

8
methyl 2-cyclopropylaminomethylene-3-(2,4,5-trifluorophenyl)-3-oxopropanoate [ No CAS ]
[ 93107-30-3 ]

References: [1]Synthesis,2006,p. 963 - 968.

9
[ 93107-30-3 ]
1-Cyclopropyl-6-fluoro-7-((S)-3-methyl-piperazin-1-yl)-4-oxo-1,4-dihydro-quinoline-3-carboxylic acid; hydrochloride [ No CAS ]

References: [1]Bioorganic and Medicinal Chemistry,2005,vol. 13,p. 2451 - 2458.

10
[ 93107-30-3 ]
1-Cyclopropyl-6-fluoro-7-((R)-3-methyl-piperazin-1-yl)-4-oxo-1,4-dihydro-quinoline-3-carboxylic acid; hydrochloride [ No CAS ]

References: [1]Bioorganic and Medicinal Chemistry,2005,vol. 13,p. 2451 - 2458.

11
[ 93107-30-3 ]
7-((3S)-amino-(4R)-ethylpiperidin-1-yl)-1-cyclopropyl-6-fluoro-4-oxo-1,4-dihydroquinoline-3-carboxylic acid dihydrochloride [ No CAS ]

References: [1]Journal of Medicinal Chemistry,2003,vol. 46,p. 3655 - 3661.

12
[ 93107-30-3 ]
1-Cyclopropyl-6-fluoro-7-((2R,3S)-2-methyl-3-methylamino-azetidin-1-yl)-4-oxo-1,4-dihydro-quinoline-3-carboxylic acid [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1994,vol. 37,p. 4195 - 4210.

13
[ 93107-30-3 ]
7-((2R,3S)-3-Aminomethyl-2-methyl-azetidin-1-yl)-1-cyclopropyl-6-fluoro-4-oxo-1,4-dihydro-quinoline-3-carboxylic acid [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1994,vol. 37,p. 4195 - 4210.

14
[ 93107-30-3 ]
1-Cyclopropyl-7-((2R,3S)-3-ethylaminomethyl-2-methyl-azetidin-1-yl)-6-fluoro-4-oxo-1,4-dihydro-quinoline-3-carboxylic acid [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1994,vol. 37,p. 4195 - 4210.

15
[ 93107-30-3 ]
[ 105112-37-6 ]

References: [1]Journal of Medicinal Chemistry,1988,vol. 31,p. 983 - 991.
[2]Journal of Heterocyclic Chemistry,1987,vol. 24,p. 181 - 185.

16
[ 101799-76-2 ]
[ 93107-30-3 ]

References: [1]Journal of Medicinal Chemistry,1988,vol. 31,p. 983 - 991.
[2]Liebigs Annalen der Chemie,1987,p. 29 - 37.
[3]Patent: US4940710,1990,A .

17
[ 93107-30-3 ]
(R)-7-[3-(1-Amino-1-methylethyl)-1-pyrrolidinyl]-1-cyclopropyl-6-fluoro-1,4-dihydro-4-oxo-3-quinolinecarboxylic acid, monohydrochloride [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1994,vol. 37,p. 733 - 738.

18
[ 93107-30-3 ]
7-[(S)-3-(1-Amino-1-methyl-ethyl)-pyrrolidin-1-yl]-1-cyclopropyl-6-fluoro-4-oxo-1,4-dihydro-quinoline-3-carboxylic acid; hydrochloride [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1994,vol. 37,p. 733 - 738.

19
[ 93107-30-3 ]
[ 103222-12-4 ]

References: [1]Arzneimittel-Forschung/Drug Research,1986,vol. 36,p. 1545 - 1549.

20
[ 93107-30-3 ]
[ 132233-67-1 ]

References: [1]Journal of Medicinal Chemistry,1993,vol. 36,p. 871 - 882.

21
[ 93107-30-3 ]
1-cyclopropyl-6-fluoro-1,4-dihydro-7-[3'-aminomethyl-1'-azetidinyl]-4-oxo-3-quinoline-carboxylic acid [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1993,vol. 36,p. 801 - 810.

22
[ 93107-30-3 ]
1-cyclopropyl-6-fluoro-7-(3-methylamino-1-azetidinyl)-1,4-dihydro-4-oxo-3-quinolinecarboxylic acid [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1993,vol. 36,p. 801 - 810.

23
[ 93107-30-3 ]
1-cyclopropyl-6-fluoro-7-(3-amino-3-methyl-1-azetidinyl)-1,4-dihydro-4-oxo-3-quinolinecarboxylic acid [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1993,vol. 36,p. 801 - 810.

24
[ 93107-30-3 ]
[ 132770-51-5 ]

References: [1]Journal of Medicinal Chemistry,1993,vol. 36,p. 801 - 810.

25
[ 93107-30-3 ]
[ 132770-06-0 ]

References: [1]Journal of Medicinal Chemistry,1993,vol. 36,p. 801 - 810.

26
[ 93107-30-3 ]
1-cyclopropyl-6-fluoro-1,4-dihydro-4-oxo-7-(3-aminomethyl-3-methyl-1-azetidinyl)-quinoline-3-carboxylic acid [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1993,vol. 36,p. 801 - 810.

27
[ 93107-30-3 ]
1-cyclopropyl-6-fluoro-7-(3-ethylaminomethyl-1-azetidinyl)-1,4-dihydro-4-oxo-3-quinolinecarboxylic acid [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1993,vol. 36,p. 801 - 810.

28
[ 93107-30-3 ]
1-cyclopropyl-6-fluoro-7-(3-ethylaminomethyl-3-methyl-1-azetidinyl)-1,4-dihydro-4-oxo-3-quinolinecarboxylic acid [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1993,vol. 36,p. 801 - 810.

29
[ 93107-30-3 ]
1-Cyclopropyl-6-fluoro-7-{3-methyl-3-[methyl-(2-oxo-propyl)-amino]-azetidin-1-yl}-4-oxo-1,4-dihydro-quinoline-3-carboxylic acid [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1993,vol. 36,p. 801 - 810.

30
[ 93107-30-3 ]
7-[(S)-3-((R)-1-Amino-ethyl)-pyrrolidin-1-yl]-1-cyclopropyl-6-fluoro-4-oxo-1,4-dihydro-quinoline-3-carboxylic acid; hydrochloride [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1993,vol. 36,p. 871 - 882.

31
[ 93107-30-3 ]
7-[(S)-3-((S)-1-Amino-ethyl)-pyrrolidin-1-yl]-1-cyclopropyl-6-fluoro-4-oxo-1,4-dihydro-quinoline-3-carboxylic acid; hydrochloride [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1993,vol. 36,p. 871 - 882.

32
[ 93107-30-3 ]
1-Cyclopropyl-6-fluoro-7-[(R)-3-((S)-1-methylamino-ethyl)-pyrrolidin-1-yl]-4-oxo-1,4-dihydro-quinoline-3-carboxylic acid; hydrofluoride [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1993,vol. 36,p. 871 - 882.

33
[ 93107-30-3 ]
7-[(R)-3-((S)-1-Amino-ethyl)-pyrrolidin-1-yl]-1-cyclopropyl-6-fluoro-4-oxo-1,4-dihydro-quinoline-3-carboxylic acid; hydrochloride [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1993,vol. 36,p. 871 - 882.

34
[ 93107-30-3 ]
7-[(R)-3-((R)-1-Amino-ethyl)-pyrrolidin-1-yl]-1-cyclopropyl-6-fluoro-4-oxo-1,4-dihydro-quinoline-3-carboxylic acid; hydrochloride [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1993,vol. 36,p. 871 - 882.

35
[ 93107-30-3 ]
1-Cyclopropyl-6-fluoro-7-[(R)-3-((R)-1-methylamino-ethyl)-pyrrolidin-1-yl]-4-oxo-1,4-dihydro-quinoline-3-carboxylic acid; hydrochloride [ No CAS ]

References: [1]Journal of Medicinal Chemistry,1993,vol. 36,p. 871 - 882.

Historical Records

Technical Information

• Alkyl Halide Occurrence • Arndt-Eistert Homologation • Baeyer-Villiger Oxidation • Barbier Coupling Reaction • Baylis-Hillman Reaction • Bucherer-Bergs Reaction • Clemmensen Reduction • Corey-Bakshi-Shibata (CBS) Reduction • Corey-Chaykovsky Reaction • Fischer Indole Synthesis • Grignard Reaction • Henry Nitroaldol Reaction • Horner-Wadsworth-Emmons Reaction • Hunsdiecker-Borodin Reaction • Hydride Reductions • Lawesson's Reagent • Leuckart-Wallach Reaction • McMurry Coupling • Meerwein-Ponndorf-Verley Reduction • Passerini Reaction • Paternò-Büchi Reaction • Petasis Reaction • Peterson Olefination • Pictet-Spengler Tetrahydroisoquinoline Synthesis • Preparation of Aldehydes and Ketones • Preparation of Amines • Preparation of Carboxylic Acids • Prins Reaction • Reactions of Aldehydes and Ketones • Reactions of Amines • Reactions of Carboxylic Acids • Reformatsky Reaction • Robinson Annulation • Schlosser Modification of the Wittig Reaction • Schmidt Reaction • Specialized Acylation Reagents-Ketenes • Stobbe Condensation • Tebbe Olefination • Ugi Reaction • Wittig Reaction • Wolff-Kishner Reduction

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[ 93107-30-3 ]

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H223	Flammable aerosol
H224	Extremely flammable liquid and vapour
H225	Highly flammable liquid and vapour
H226	Flammable liquid and vapour
H227	Combustible liquid
H228	Flammable solid
H229	Pressurized container: may burst if heated
H230	May react explosively even in the absence of air
H231	May react explosively even in the absence of air at elevated pressure and/or temperature
H240	Heating may cause an explosion
H241	Heating may cause a fire or explosion
H242	Heating may cause a fire
H250	Catches fire spontaneously if exposed to air
H251	Self-heating; may catch fire
H252	Self-heating in large quantities; may catch fire
H260	In contact with water releases flammable gases which may ignite spontaneously
H261	In contact with water releases flammable gas
H270	May cause or intensify fire; oxidizer
H271	May cause fire or explosion; strong oxidizer
H272	May intensify fire; oxidizer
H280	Contains gas under pressure; may explode if heated
H281	Contains refrigerated gas; may cause cryogenic burns or injury
H290	May be corrosive to metals
Health hazards
Code	Phrase
H300	Fatal if swallowed
H301	Toxic if swallowed
H302	Harmful if swallowed
H303	May be harmful if swallowed
H304	May be fatal if swallowed and enters airways
H305	May be harmful if swallowed and enters airways
H310	Fatal in contact with skin
H311	Toxic in contact with skin
H312	Harmful in contact with skin
H313	May be harmful in contact with skin
H314	Causes severe skin burns and eye damage
H315	Causes skin irritation
H316	Causes mild skin irritation
H317	May cause an allergic skin reaction
H318	Causes serious eye damage
H319	Causes serious eye irritation
H320	Causes eye irritation
H330	Fatal if inhaled
H331	Toxic if inhaled
H332	Harmful if inhaled
H333	May be harmful if inhaled
H334	May cause allergy or asthma symptoms or breathing difficulties if inhaled
H335	May cause respiratory irritation
H336	May cause drowsiness or dizziness
H340	May cause genetic defects
H341	Suspected of causing genetic defects
H350	May cause cancer
H351	Suspected of causing cancer
H360	May damage fertility or the unborn child
H361	Suspected of damaging fertility or the unborn child
H361d	Suspected of damaging the unborn child
H362	May cause harm to breast-fed children
H370	Causes damage to organs
H371	May cause damage to organs
H372	Causes damage to organs through prolonged or repeated exposure
H373	May cause damage to organs through prolonged or repeated exposure
Environmental hazards
Code	Phrase
H400	Very toxic to aquatic life
H401	Toxic to aquatic life
H402	Harmful to aquatic life
H410	Very toxic to aquatic life with long-lasting effects
H411	Toxic to aquatic life with long-lasting effects
H412	Harmful to aquatic life with long-lasting effects
H413	May cause long-lasting harmful effects to aquatic life
H420	Harms public health and the environment by destroying ozone in the upper atmosphere

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CAS No.: 93107-30-3

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