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Chemical Structure| 91626-53-8 Chemical Structure| 91626-53-8
Chemical Structure| 91626-53-8

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1-(4-Chloro-3-(trifluoromethyl)phenyl)hydrazine

CAS No.: 91626-53-8

4.5 *For Research Use Only !

Cat. No.: A354532 Purity: 95%

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Product Details of [ 91626-53-8 ]

CAS No. :91626-53-8
Formula : C7H6ClF3N2
M.W : 210.58
SMILES Code : NNC1=CC=C(Cl)C(C(F)(F)F)=C1
MDL No. :MFCD02656466

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Application In Synthesis [ 91626-53-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 91626-53-8 ]

[ 91626-53-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 320-50-3 ]
  • [ 91626-53-8 ]
YieldReaction ConditionsOperation in experiment
12.1 g With pyridine; hydrazine hydrate; In dichloromethane; ethyl acetate; at 130.0℃; for 4.0h;Autoclave; Take 2,5-dichloro-3-trifluoromethylbenzene 6 (15.4 g) in an autoclave,Hydrazine hydrate (26g) and pyridine (150ml) were added together with ethyl acetate and methylene chloride (250ml) as organic solvents. The mixture was heated to 130C and reacted for 4 hours. After cooling, excess hydrazine was removed, vacuum distillation was performed, and the residue was added with solvent petroleum. The ether is recrystallized to give 2-chloro-3-trifluoromethylphenylhydrazine 7 (12.1 g)
 

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